Technology Process of C40H58S2Si2
There total 4 articles about C40H58S2Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NIS / CHCl3; acetic acid
2: NEt3; CuI; PPh3 / Pd(OAc)2 / dimethylformamide
With
N-iodo-succinimide; copper(l) iodide; triethylamine; triphenylphosphine;
palladium diacetate;
In
chloroform; acetic acid; N,N-dimethyl-formamide;
2: Sonogashira coupling;
DOI:10.1246/cl.2005.724
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 89 percent / 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene chloride / Pd2(dba)3
2: NIS / CHCl3; acetic acid
3: NEt3; CuI; PPh3 / Pd(OAc)2 / dimethylformamide
With
N-iodo-succinimide; copper(l) iodide; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride; triethylamine; triphenylphosphine;
palladium diacetate; tris(dibenzylideneacetone)dipalladium (0);
In
chloroform; acetic acid; N,N-dimethyl-formamide;
1: Kumada coupling / 3: Sonogashira coupling;
DOI:10.1246/cl.2005.724
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 89 percent / 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene chloride / Pd2(dba)3
2: NIS / CHCl3; acetic acid
3: NEt3; CuI; PPh3 / Pd(OAc)2 / dimethylformamide
With
N-iodo-succinimide; copper(l) iodide; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride; triethylamine; triphenylphosphine;
palladium diacetate; tris(dibenzylideneacetone)dipalladium (0);
In
chloroform; acetic acid; N,N-dimethyl-formamide;
1: Kumada coupling / 3: Sonogashira coupling;
DOI:10.1246/cl.2005.724
