Technology Process of C34H26O6
There total 9 articles about C34H26O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 24h;
DOI:10.1002/ejoc.201001442
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium carbonate / methanol / 20 °C
2: N-Bromosuccinimide; silver nitrate / acetone / 1.5 h / 20 °C
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; hydrogen; triethylamine / tetrahydrofuran / 2 h / 20 °C
4: N-Bromosuccinimide; silver fluoride / acetonitrile / 1.5 h / 20 °C
5: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; hydrogen; triethylamine / tetrahydrofuran / 2 h / 20 °C
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / -78 °C
7: copper(l) iodide / N,N-dimethyl-formamide / 24 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; tetrabutyl ammonium fluoride; hydrogen; silver fluoride; potassium carbonate; silver nitrate; triethylamine;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; acetonitrile;
3: Sonogashira coupling / 5: Sonogashira coupling;
DOI:10.1002/ejoc.201001442
- Guidance literature:
-
Multi-step reaction with 7 steps
1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
2: N-Bromosuccinimide; silver nitrate / acetone / 1.5 h / 20 °C
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; hydrogen; triethylamine / tetrahydrofuran / 2 h / 20 °C
4: N-Bromosuccinimide; silver fluoride / acetonitrile / 1.5 h / 20 °C
5: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; hydrogen; triethylamine / tetrahydrofuran / 2 h / 20 °C
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / -78 °C
7: copper(l) iodide / N,N-dimethyl-formamide / 24 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; tetrabutyl ammonium fluoride; hydrogen; silver fluoride; silver nitrate; triethylamine; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetone; acetonitrile;
3: Sonogashira coupling / 5: Sonogashira coupling;
DOI:10.1002/ejoc.201001442