tetrakis(trimethylphosphine)(2,6-diisopropylphenyloxy)hydridomolybdenum

Base Information

Chemical Name:tetrakis(trimethylphosphine)(2,6-diisopropylphenyloxy)hydridomolybdenum
CAS No.:181479-61-8
Molecular Formula:C₂₄H₅₄MoOP₄
Molecular Weight:578.527
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Chemical Property of tetrakis(trimethylphosphine)(2,6-diisopropylphenyloxy)hydridomolybdenum

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Technology Process of tetrakis(trimethylphosphine)(2,6-diisopropylphenyloxy)hydridomolybdenum

There total 1 articles about tetrakis(trimethylphosphine)(2,6-diisopropylphenyloxy)hydridomolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 82456-09-5
hexakis(trimethylphosphine)molybdenum

: 2078-54-8
2,6-diisopropylphenol

: 181479-61-8
tetrakis(trimethylphosphine)(2,6-diisopropylphenyloxy)hydridomolybdenum

Guidance literature:: In benzene; under Ar, Schlenk techniques; mixt. of Mo complex and 2,6-diisopropylphenol (molar ratio 1.1:1) in benzene stirred at 60°C for 1.5 h; volatiles removed under reduced pressure; extd. into pentane; filtrate concd.; cooled to -78°C; filtered; solid dried in vac.; elem. anal.;
DOI:10.1016/S0022-328X(02)01306-2