Technology Process of C26H38O6Si
There total 12 articles about C26H38O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: zinc(II) tetrahydroborate / diethyl ether / -78 - -30 °C
2: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 0 - 24 °C
3: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0 - 24 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C
5: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C
6: 2,6-dimethylpyridine / dichloromethane / -40 °C
7: methanol; potassium carbonate / -15 °C
With
2,6-dimethylpyridine; methanol; tert.-butylhydroperoxide; lithium aluminium tetrahydride; zinc(II) tetrahydroborate; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2011.08.051
- Guidance literature:
-
Multi-step reaction with 9 steps
1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 25 °C
2: tert.-butyl lithium / tetrahydrofuran / -78 °C
3: zinc(II) tetrahydroborate / diethyl ether / -78 - -30 °C
4: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 0 - 24 °C
5: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0 - 24 °C
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C
7: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C
8: 2,6-dimethylpyridine / dichloromethane / -40 °C
9: methanol; potassium carbonate / -15 °C
With
2,6-dimethylpyridine; methanol; tert.-butylhydroperoxide; dmap; lithium aluminium tetrahydride; zinc(II) tetrahydroborate; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2011.08.051
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C
3: 2,6-dimethylpyridine / dichloromethane / -40 °C
4: methanol; potassium carbonate / -15 °C
With
2,6-dimethylpyridine; methanol; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; potassium carbonate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.08.051