Technology Process of 6--6-mercapto-1-hexanol
There total 8 articles about 6--6-mercapto-1-hexanol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol;
for 3h;
Heating;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 87 percent / fuming nitric acid / 4 h / 0 °C
2: 77 percent / ethyldiisopropylamine / CH2Cl2 / Ambient temperature
With
nitric acid; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 57 percent / sodium iodide, sodium bicarbonate / acetone / 3.5 h / Heating
2: 70 percent / sodium hydrogen sulfide / methanol / 3 h
3: 77 percent / ethyldiisopropylamine / CH2Cl2 / Ambient temperature
With
sodium hydrogensulfide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; sodium iodide;
In
methanol; dichloromethane; acetone;
