C₁₈H₁₇NO₂

Base Information

• Chemical Name: C₁₈H₁₇NO₂
• CAS No.: 91606-57-4
• Molecular Formula: C₁₈H₁₇NO₂
• Molecular Weight: 279.338
• Mol file: 91606-57-4.mol

Synonyms:

Chemical Property of C₁₈H₁₇NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₁₇NO₂

There total 4 articles about C₁₈H₁₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-<1-(Trimethylsilyl)cyclopropyl>-2-cyclopropylideneethanol (91606-52-9) → C18H17NO2 (91606-57-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / SOCl₂ / diethyl ether / 0.5 h / 0 °C

2: 90 percent / tetra-n-butylammonium fluoride / dimethylsulfoxide / 24 h / Ambient temperature

3: benzene / Heating

With thionyl chloride; tetrabutyl ammonium fluoride; In diethyl ether; dimethyl sulfoxide; benzene;

DOI:10.1021/jo00193a032

Reference yield:

trans-1-(1-Chlorocyclopropyl)-2-<1-(trimethylsilyl)cyclopropyl>ethylene (91606-53-0) → C18H17NO2 (91606-57-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / tetra-n-butylammonium fluoride / dimethylsulfoxide / 24 h / Ambient temperature

2: benzene / Heating

With tetrabutyl ammonium fluoride; In dimethyl sulfoxide; benzene;

DOI:10.1021/jo00193a032

Reference yield:

trans-1,2-Bis<1-(trimethylsilyl)cyclopropyl>ethylene Oxide (91606-51-8) → C18H17NO2 (91606-57-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 65 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 12 h / Heating

2: 85 percent / SOCl₂ / diethyl ether / 0.5 h / 0 °C

3: 90 percent / tetra-n-butylammonium fluoride / dimethylsulfoxide / 24 h / Ambient temperature

4: benzene / Heating

With thionyl chloride; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; benzene;

DOI:10.1021/jo00193a032

upstream raw materials:

N-phenyl-maleimide

Dicyclopropylideneethane

1-<1-(Trimethylsilyl)cyclopropyl>-2-cyclopropylideneethanol

trans-1-(1-Chlorocyclopropyl)-2-<1-(trimethylsilyl)cyclopropyl>ethylene