C₂₀H₂₄N₂O₃

Base Information

Chemical Name:C₂₀H₂₄N₂O₃
CAS No.:1374967-29-9
Molecular Formula:C₂₀H₂₄N₂O₃
Molecular Weight:340.422
Hs Code.:

C<sub>20</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₀H₂₄N₂O₃

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Technology Process of C₂₀H₂₄N₂O₃

There total 6 articles about C₂₀H₂₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1374967-29-9
C₂₀H₂₄N₂O₃

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.333333h;

In tetrahydrofuran; toluene; Further stages;

Reference yield:

: 919-93-7
3,3-dimethylpent-4-enal

: 1374967-19-7
C₁₃H₁₄N₂O₃

: C₂₀H₂₄N₂O₃

: 1374967-29-9
C₂₀H₂₄N₂O₃

Guidance literature:: C₁₃H₁₄N₂O₃; With lithium hexamethyldisilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.25h; Inert atmosphere;

3,3-dimethylpent-4-enal; In tetrahydrofuran; toluene; at -78 ℃; for 0.25h; optical yield given as %de; diastereoselective reaction; Further stages; Inert atmosphere;
DOI:10.1021/ol3007056

Reference yield:

: 366003-57-8
(+)-(2S)-methyl 2-(2-chloroacetylamino)-3-hydroxypropanoate

: C₂₀H₂₄N₂O₃

: 1374967-29-9
C₂₀H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 16 h / Inert atmosphere; Reflux

2.1: sodium azide / butanone / 15 h / 80 °C / Inert atmosphere

3.1: resin-bound triphenyl phosphine / toluene / 20 h / 90 °C / Inert atmosphere

4.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C / Inert atmosphere

4.2: 0.25 h / -78 °C / Inert atmosphere

With sodium azide; toluene-4-sulfonic acid; lithium hexamethyldisilazane; In tetrahydrofuran; toluene; butanone; 3.1: Staudinger reaction;
DOI:10.1021/ol3007056