1,N¹-(3-oxapentamethylene)-N²-4-nitrophenyl>amidinoyl isothiocyanate

Base Information

• Chemical Name: 1,N¹-(3-oxapentamethylene)-N²-4-nitrophenyl>amidinoyl isothiocyanate
• CAS No.: 49573-72-0
• Molecular Formula: C₁₂H₁₂N₄O₃S
• Molecular Weight: 292.318

Synonyms:

Chemical Property of 1,N¹-(3-oxapentamethylene)-N²-4-nitrophenyl>amidinoyl isothiocyanate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of 1,N¹-(3-oxapentamethylene)-N²-4-nitrophenyl>amidinoyl isothiocyanate

There total 1 articles about 1,N¹-(3-oxapentamethylene)-N²-4-nitrophenyl>amidinoyl isothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-nitro-phenyl)-morpholine-4-carboximidoyl chloride (94628-03-2) + ammonium thiocyanate (1147550-11-5) → N-(4-nitro-phenyl)-morpholine-4-carboximidoyl isothiocyanate (49573-72-0)

Guidance literature:

DOI:10.1016/0040-4020(73)80080-8

Reference yield: 60.0%

1,N1-(3-oxapentamethylene)-N2-4-nitrophenyl>amidinoyl isothiocyanate (49573-72-0) + p-nitrophenyl isothiocyanate (2131-61-5) → (2-Morpholin-4-yl-6-nitro-quinazolin-4-yl)-(4-nitro-phenyl)-amine (75426-62-9)

Guidance literature:

In N,N-dimethyl-formamide; for 1h; Heating;

Reference yield: 30.0%

1,N1-(3-oxapentamethylene)-N2-4-nitrophenyl>amidinoyl isothiocyanate (49573-72-0) → 2-morpholin-4-yl-6-nitro-3H-quinazoline-4-thione + (2-Morpholin-4-yl-6-nitro-quinazolin-4-yl)-(4-nitro-phenyl)-amine (75426-62-9)

Guidance literature:

In acetonitrile; for 5h; Heating;

upstream raw materials:

N-(4-nitro-phenyl)-morpholine-4-carboximidoyl chloride

ammonium thiocyanate

Downstream raw materials:

morpholine-4-carbothioic acid [N-(4-nitro-phenyl)-morpholine-4-carboximidoyl]-amide

2-(4-nitro-anilino)-thiazolo[3,2-a][1,3,5]triazine-4-thione

N-(4-nitro-phenyl)-morpholine-4-carboximidic acid (butyl-thiocarbamoyl)-amide

N-(4-nitro-phenyl)-morpholine-4-carboximidic acid (phenyl-thiocarbamoyl)-amide

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