(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate

Base Information

Chemical Name:(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate
CAS No.:944479-63-4
Molecular Formula:C₄₆H₄₈F₁₇N₅O₅
Molecular Weight:1073.89
Hs Code.:

(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate

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Chemical Property of (2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate

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Technology Process of (2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate

There total 7 articles about (2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 944479-39-4
(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate

: 944479-63-4
(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0.08 h / 120 °C / microwave irradiation

2: 72 mg / tetrahydrofuran; H₂O / 0.17 h / 120 °C / microwave irradiation

3: 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

With dmap; In tetrahydrofuran; dichloromethane; water; 1: Staudinger reaction;
DOI:10.1016/j.tet.2007.03.034

Reference yield:

: 944479-30-5
(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-azido-2,5-dimethylhexanoate

: 944479-63-4
(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 0.08 h / 120 °C / microwave irradiation

2: 100 percent / tetrahydrofuran; H₂O / 0.17 h / 120 °C / microwave irradiation

3: 84 mg / 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

4: tetrahydrofuran / 0.08 h / 120 °C / microwave irradiation

5: 72 mg / tetrahydrofuran; H₂O / 0.17 h / 120 °C / microwave irradiation

6: 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

With dmap; In tetrahydrofuran; dichloromethane; water; 1: Staudinger reaction / 4: Staudinger reaction;
DOI:10.1016/j.tet.2007.03.034

Reference yield:

: C₅₄H₅₂F₁₇N₂O₄P

: 944479-63-4
(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2R,3S)-3-((2R,3S)-3-azido-2-methyl-3-phenylpropanamido)-2-methyl-3-phenylpropanamido)-2,5-dimethylhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 72 mg / tetrahydrofuran; H₂O / 0.17 h / 120 °C / microwave irradiation

2: 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

With dmap; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tet.2007.03.034