C₄₄H₂₄Br₂Cl₂N₄Ni

Base Information

• Chemical Name: C₄₄H₂₄Br₂Cl₂N₄Ni
• CAS No.: 1539327-07-5
• Molecular Formula: C₄₄H₂₄Br₂Cl₂N₄Ni
• Molecular Weight: 898.105
• Mol file: 1539327-07-5.mol

Synonyms:

Chemical Property of C₄₄H₂₄Br₂Cl₂N₄Ni

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₄₄H₂₄Br₂Cl₂N₄Ni

There total 2 articles about C₄₄H₂₄Br₂Cl₂N₄Ni which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

C44H26Br2Cl2N4 + nickel diacetate (373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6) → C44H24Br2Cl2N4Ni (1539327-07-5)

Guidance literature:

In methanol; N,N-dimethyl-formamide; Reflux;

DOI:10.1139/cjc-2013-0400

Reference yield:

2,2'-((4-chlorophenyl)methylene)bis(1H-pyrrole) (137018-26-9) → C44H24Br2Cl2N4Ni (1539327-07-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide; methanol / Reflux

With trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1139/cjc-2013-0400

upstream raw materials:

nickel diacetate

2,2'-((4-chlorophenyl)methylene)bis(1H-pyrrole)