C₂₆H₃₀BrCl₃N₂O₆

Base Information

Chemical Name:C₂₆H₃₀BrCl₃N₂O₆
CAS No.:1452587-19-7
Molecular Formula:C₂₆H₃₀BrCl₃N₂O₆
Molecular Weight:652.797
Hs Code.:

C<sub>26</sub>H<sub>30</sub>BrCl<sub>3</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:

Suppliers and Price of C₂₆H₃₀BrCl₃N₂O₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₆H₃₀BrCl₃N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₆H₃₀BrCl₃N₂O₆

There total 5 articles about C₂₆H₃₀BrCl₃N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1452587-19-7
C₂₆H₃₀BrCl₃N₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1: chlorine / acetic acid; water

2: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

3: bromine / chloroform / 2 h / 20 °C

4: chloroform / 18 h / 20 °C

5: hydrogen bromide; water / methanol / 48 h

6: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h

With water; hydrogen bromide; bromine; chlorine; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; chloroform; water; acetic acid; N,N-dimethyl-formamide; 4: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 17044-70-1
3',5'-dichloro-4'-hydroxyacetophenone

: 1452587-19-7
C₂₆H₃₀BrCl₃N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

2: bromine / chloroform / 2 h / 20 °C

3: chloroform / 18 h / 20 °C

4: hydrogen bromide; water / methanol / 48 h

5: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h

With water; hydrogen bromide; bromine; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; chloroform; N,N-dimethyl-formamide; 3: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 1452587-06-2
C₁₁H₁₁BrCl₂O₂

: 1452587-19-7
C₂₆H₃₀BrCl₃N₂O₆

Guidance literature:: Multi-step reaction with 4 steps

1: bromine / chloroform / 2 h / 20 °C

2: chloroform / 18 h / 20 °C

3: hydrogen bromide; water / methanol / 48 h

4: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h

With water; hydrogen bromide; bromine; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; chloroform; N,N-dimethyl-formamide; 2: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2013.07.017