Technology Process of C43H63N3O10Si2
There total 9 articles about C43H63N3O10Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hexamethylsilazane;
In
tetrahydrofuran; toluene;
at 0 ℃;
for 2h;
stereoselective reaction;
DOI:10.1021/jo201935w
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoroacetic acid / tetrahydrofuran; water / 7 h / 0 °C
1.2: pH 9
2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / acetonitrile / 0.75 h / 80 °C
3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C
3.2: 17 h / -78 - 20 °C
4.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 2 h / 0 °C
With
potassium hexamethylsilazane; trifluoroacetic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; water; toluene; acetonitrile;
3.2: Wittig-Horner reaction;
DOI:10.1021/jo201935w
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C
1.2: 17 h / -78 - 20 °C
2.1: tetra-(n-butyl)ammonium iodide; sodium carbonate / dichloromethane; water / 18 h / 20 °C
3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 2 h / 0 °C
With
tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium carbonate;
In
tetrahydrofuran; dichloromethane; water; toluene;
1.2: Wittig-Horner reaction;
DOI:10.1021/jo201935w
