1ALPHA-DEOXY-1ALPHA-AZIDO-4ALPHA-DEOXY-4ALPHA-(THYMIN-1-YL)-2,3ALPHA:2ALPHA,5ALPHA-DIANHYDRO-L-ALTRITOL

Base Information

Chemical Name:1ALPHA-DEOXY-1ALPHA-AZIDO-4ALPHA-DEOXY-4ALPHA-(THYMIN-1-YL)-2,3ALPHA:2ALPHA,5ALPHA-DIANHYDRO-L-ALTRITOL
CAS No.:900513-69-1
Molecular Formula:C₁₁H₁₃N₅O₄
Molecular Weight:279.255
Hs Code.:
Mol file:900513-69-1.mol

Synonyms:1ALPHA-DEOXY-1ALPHA-AZIDO-4ALPHA-DEOXY-4ALPHA-(THYMIN-1-YL)-2,3ALPHA:2ALPHA,5ALPHA-DIANHYDRO-L-ALTRITOL;1′-Deoxy-1′-azido-4′-deoxy-4′-(thyMin-1-yl)- 2,3′:2′,5′-dianhydro-L-altritol

Suppliers and Price of 1ALPHA-DEOXY-1ALPHA-AZIDO-4ALPHA-DEOXY-4ALPHA-(THYMIN-1-YL)-2,3ALPHA:2ALPHA,5ALPHA-DIANHYDRO-L-ALTRITOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1'-DEOXY-1'-AZIDO-4'-DEOXY-4'-(THYMIN-1-YL)-2,3',2',5'-DIANHYDRO-L-ALTRITOL 95.00%
5MG
$ 497.77

Total 2 raw suppliers

Chemical Property of 1ALPHA-DEOXY-1ALPHA-AZIDO-4ALPHA-DEOXY-4ALPHA-(THYMIN-1-YL)-2,3ALPHA:2ALPHA,5ALPHA-DIANHYDRO-L-ALTRITOL

Chemical Property:

PSA：123.33000
LogP:-0.62344

Purity/Quality:

99% ^*data from raw suppliers

1'-DEOXY-1'-AZIDO-4'-DEOXY-4'-(THYMIN-1-YL)-2,3',2',5'-DIANHYDRO-L-ALTRITOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1ALPHA-DEOXY-1ALPHA-AZIDO-4ALPHA-DEOXY-4ALPHA-(THYMIN-1-YL)-2,3ALPHA:2ALPHA,5ALPHA-DIANHYDRO-L-ALTRITOL

There total 2 articles about 1ALPHA-DEOXY-1ALPHA-AZIDO-4ALPHA-DEOXY-4ALPHA-(THYMIN-1-YL)-2,3ALPHA:2ALPHA,5ALPHA-DIANHYDRO-L-ALTRITOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 900513-64-6
6'-O-benzoyl-1'-deoxy-1'-azido-4'-deoxy-4'-(thymin-1-yl)-2,3':2',5'-dianhydro-L-altritol

: 900513-69-1
1'-deoxy-1'-azido-4'-deoxy-4'-(thymin-1-yl)-2,3':2',5'-dianhydro-L-altritol

Guidance literature:: With methylamine; In methanol; at 20 ℃; for 0.25h;
DOI:10.1016/j.tetasy.2006.03.034

Reference yield:

: 258524-62-8
2,5-anhydro-1-O-benzoyl-3-deoxy-3-(thymin-1-yl)-L-mannitol

: 900513-69-1
1'-deoxy-1'-azido-4'-deoxy-4'-(thymin-1-yl)-2,3':2',5'-dianhydro-L-altritol

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; sodium azide; carbon tetrabromide / dimethylformamide / 36 h / 20 °C

1.2: 83 percent / dimethylformamide; methanol / 1 h

2.1: 98 percent / methylamine / methanol / 0.25 h / 20 °C

With sodium azide; carbon tetrabromide; triphenylphosphine; methylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2006.03.034