2,5-ANHYDRO-3-DEOXY-3-(3,4-DIHYDRO-2,4-DIOXO-1(2H)-PYRIMIDINYL)-D-IDITOL

Base Information

Chemical Name:2,5-ANHYDRO-3-DEOXY-3-(3,4-DIHYDRO-2,4-DIOXO-1(2H)-PYRIMIDINYL)-D-IDITOL
CAS No.:302790-86-9
Molecular Formula:C10H14N2O6
Molecular Weight:258.229
Hs Code.:
Mol file:302790-86-9.mol

Synonyms:2,5-ANHYDRO-3-DEOXY-3-(3,4-DIHYDRO-2,4-DIOXO-1(2H)-PYRIMIDINYL)-D-IDITOL

Suppliers and Price of 2,5-ANHYDRO-3-DEOXY-3-(3,4-DIHYDRO-2,4-DIOXO-1(2H)-PYRIMIDINYL)-D-IDITOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,5-ANHYDRO-3-DEOXY-3-(3,4-DIHYDRO-2,4-DIOXO-1(2H)-PYRIMIDINYL)-D-IDITOL 95.00%
5MG
$ 505.82

Total 1 raw suppliers

Chemical Property of 2,5-ANHYDRO-3-DEOXY-3-(3,4-DIHYDRO-2,4-DIOXO-1(2H)-PYRIMIDINYL)-D-IDITOL

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:: 2,5-ANHYDRO-3-DEOXY-3-(3,4-DIHYDRO-2,4-DIOXO-1(2H)-PYRIMIDINYL)-D-IDITOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,5-ANHYDRO-3-DEOXY-3-(3,4-DIHYDRO-2,4-DIOXO-1(2H)-PYRIMIDINYL)-D-IDITOL

There total 13 articles about 2,5-ANHYDRO-3-DEOXY-3-(3,4-DIHYDRO-2,4-DIOXO-1(2H)-PYRIMIDINYL)-D-IDITOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 91318-12-6
2,5:3,4-dianhydro-1,6-di-O-benzoyl-D-altritol

: 66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6
uracil

: 196596-87-9,302790-82-5,302790-86-9
3-deoxy-3-(uracil-1'-yl)-2,5-anhydro-D-mannitol

: 196596-87-9,302790-82-5,302790-86-9
4-deoxy-4-(uracil-1'-yl)-2,5-anhydro-D-iditol

Guidance literature:: 2,5:3,4-dianhydro-1,6-di-O-benzoyl-D-altritol; uracil; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 90 ℃; for 24h;

With sodium methylate; In methanol; for 3h;
DOI:10.1016/S0957-4166(00)00246-9

Reference yield: 65.0%

: 91318-12-6
2,5:3,4-dianhydro-1,6-di-O-benzoyl-D-altritol

: 66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6
uracil

: 196596-87-9,302790-82-5,302790-86-9
3-deoxy-3-(uracil-1'-yl)-2,5-anhydro-D-mannitol

: 196596-87-9,302790-82-5,302790-86-9
4-deoxy-4-(uracil-1'-yl)-2,5-anhydro-D-iditol

Guidance literature:: 2,5:3,4-dianhydro-1,6-di-O-benzoyl-D-altritol; uracil; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 90 ℃; for 24h;

With sodium methylate; In methanol; for 3h;
DOI:10.1016/S0957-4166(00)00246-9

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 196596-87-9,302790-82-5,302790-86-9
3-deoxy-3-(uracil-1'-yl)-2,5-anhydro-D-mannitol

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaNO₂; conc. HCl / H₂O / 5 h / 0 °C

2.1: NaBH₄ / H₂O / 24 h / 20 °C

3.1: pyridine / CH₂Cl₂ / 6 h / 0 °C

4.1: 90 percent / PPh₃; diethyl azodicarboxylate / dioxane / 2 h / 70 °C

5.1: DBU / dimethylformamide / 24 h / 90 °C

5.2: 65 percent / NaOMe / methanol / 3 h

With pyridine; hydrogenchloride; sodium tetrahydroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; sodium nitrite; diethylazodicarboxylate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; 1.1: Deamination / 2.1: Reduction / 3.1: Acylation / 4.1: intramolecular Mitsunobu reaction / 5.1: Ring cleavage / 5.2: methanolysis;
DOI:10.1016/S0957-4166(00)00246-9