(3-Acetylthiophen-2-yl)boronic acid

Base Information

Chemical Name:(3-Acetylthiophen-2-yl)boronic acid
CAS No.:36155-75-6
Molecular Formula:C6H7BO3S
Molecular Weight:169.99
Hs Code.:2934999090
ChEMBL ID:CHEMBL1867951
DSSTox Substance ID:DTXSID80587869
Nikkaji Number:J1.983.837D
Wikidata:Q82480352
Mol file:36155-75-6.mol

Synonyms:(3-Acetylthiophen-2-yl)boronic acid;36155-75-6;3-ACETYL-2-THIOPHENEBORONIC ACID;3-ACETYLTHIOPHEN-2-YLBORONIC ACID;SCHEMBL3788448;CHEMBL1867951;DTXSID80587869;(3-Acetylthiophen-2-yl)boronicacid;AKOS006310993;NCGC00092006-01;DB-069330

Suppliers and Price of (3-Acetylthiophen-2-yl)boronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
3-ACETYL-2-THIOPHENEBORONICACID 95
2g
$ 2475.00

Labseeker
3-ACETYL-2-THIOPHENEBORONICACID 95
1g
$ 1417.00

Crysdot
(3-Acetylthiophen-2-yl)boronicacid 95+%
1g
$ 1195.00

American Custom Chemicals Corporation
3-ACETYLTHIOPHENE-2-BORONIC ACID 95.00%
5MG
$ 502.51

American Custom Chemicals Corporation
3-ACETYLTHIOPHENE-2-BORONIC ACID 95.00%
1G
$ 2355.15

Alichem
(3-Acetylthiophen-2-yl)boronicacid
1g
$ 1036.80

Total 13 raw suppliers

Chemical Property of (3-Acetylthiophen-2-yl)boronic acid

Chemical Property:

PSA：85.77000
LogP:-0.36950
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:170.0208954
Heavy Atom Count:11
Complexity:162

Purity/Quality:

99% ^*data from raw suppliers

3-ACETYL-2-THIOPHENEBORONICACID 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B(C1=C(C=CS1)C(=O)C)(O)O

Technology Process of (3-Acetylthiophen-2-yl)boronic acid

There total 1 articles about (3-Acetylthiophen-2-yl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24287-92-1
2-Bromo-3-iodothiophene

: 108-24-7
acetic anhydride

: 36155-75-6
3-acetyl-2-thienylboronic acid

Guidance literature:: 2-Bromo-3-iodothiophene; With ethylmagnesium chloride; In tetrahydrofuran; at 15 ℃; for 0.25h;

acetic anhydride; In tetrahydrofuran; at 20 - 25 ℃; for 0.75h;

With pinacol borane; bis(tri-t-butylphosphine)palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; at 40 ℃; for 1h;
DOI:10.1021/jo034919n

Reference yield:

: 36155-75-6
3-acetyl-2-thienylboronic acid

: 4,7-Dimethyl-7,6-borazarothieno<3,2-c>-pyridin

Guidance literature:: Multi-step reaction with 2 steps

1: aq. N₂H₄ / ethanol

2: (i) nBuOH, (ii) /BRN= 1209226/, Et₂O

With hydrazine hydrate; In ethanol;