6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexyl 3-(triethoxysilyl)-propylcarbamate

Base Information

Chemical Name:6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexyl 3-(triethoxysilyl)-propylcarbamate
CAS No.:1388814-81-0
Molecular Formula:C₆₄H₆₇NO₅S₂Si
Molecular Weight:1022.46
Hs Code.:

6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexyl 3-(triethoxysilyl)-propylcarbamate

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Chemical Property of 6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexyl 3-(triethoxysilyl)-propylcarbamate

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Technology Process of 6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexyl 3-(triethoxysilyl)-propylcarbamate

There total 3 articles about 6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexyl 3-(triethoxysilyl)-propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1388814-80-9
6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexan-1-ol

: 24801-88-5
3-(triethoxypropyl) isocyanate

: 1388814-81-0
6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexyl 3-(triethoxysilyl)-propylcarbamate

Guidance literature:: With dibutyltin dilaurate; In tetrahydrofuran; at 65 ℃; for 3h; Inert atmosphere;
DOI:10.1021/la3020942

Reference yield:

: 710338-92-4
2-ethynyl-5-hexylthiophene

: 1388814-81-0
6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexyl 3-(triethoxysilyl)-propylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; diisopropylamine / tetrahydrofuran / 6 h / 80 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; diisopropylamine / tetrahydrofuran / 6 h / 80 °C

3: dibutyltin dilaurate / tetrahydrofuran / 3 h / 65 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; dibutyltin dilaurate; triethylamine; diisopropylamine; In tetrahydrofuran;
DOI:10.1021/la3020942

Reference yield:

: 1192182-18-5
2,6-dibromo-9,10-bis(2-phenylethynyl)anthracene

: 1388814-81-0
6-(5-((6-((5-hexylthiophen-2-yl)ethynyl)-9,10-bis(phenylethynyl)-anthracen-2-yl)ethynyl) thiophen-2-yl)hexyl 3-(triethoxysilyl)-propylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; diisopropylamine / tetrahydrofuran / 6 h / 80 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; diisopropylamine / tetrahydrofuran / 6 h / 80 °C

3: dibutyltin dilaurate / tetrahydrofuran / 3 h / 65 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; dibutyltin dilaurate; triethylamine; diisopropylamine; In tetrahydrofuran;
DOI:10.1021/la3020942