C₅₅H₇₀N₂O₂

Base Information

Chemical Name:C₅₅H₇₀N₂O₂
CAS No.:1425933-16-9
Molecular Formula:C₅₅H₇₀N₂O₂
Molecular Weight:791.173
Hs Code.:

C<sub>55</sub>H<sub>70</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₅H₇₀N₂O₂

Chemical Property:

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Technology Process of C₅₅H₇₀N₂O₂

There total 6 articles about C₅₅H₇₀N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 24544-04-5
2,6-diisopropylbenzenamine

: 1425933-11-4,1425934-70-8
C₃₁H₃₆O₄

: 1425933-16-9,1425934-71-9,1425969-92-1
C₅₅H₇₀N₂O₂

Guidance literature:: With toluene-4-sulfonic acid; In methanol;
DOI:10.1021/ja4004816

Reference yield:

: 914225-37-9
C₁₂H₁₇BrO₂

: 1425933-16-9,1425934-71-9,1425969-92-1
C₅₅H₇₀N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butyl lithium / tetrahydrofuran / 1 h / 20 °C / Schlenk technique; Glovebox; Cooling

1.2: 1 h / Cooling; Schlenk technique; Glovebox

1.3: 96 h / 70 °C / Schlenk technique; Glovebox; Sealed tube

2.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran / 4 h / Schlenk technique; Glovebox; Cooling

2.2: 10 h / Schlenk technique; Glovebox; Cooling

3.1: hydrogenchloride / water; methanol / 2 h / Reflux

4.1: toluene-4-sulfonic acid / methanol

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; water; 1.3: |Negishi Coupling;
DOI:10.1021/ja4004816

Reference yield:

: 6942-99-0
2,4-dibromomesitylene

: 1425933-16-9,1425934-71-9,1425969-92-1
C₅₅H₇₀N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butyl lithium / tetrahydrofuran / 1 h / 20 °C / Schlenk technique; Glovebox; Cooling

1.2: 1 h / Cooling; Schlenk technique; Glovebox

1.3: 96 h / 70 °C / Schlenk technique; Glovebox; Sealed tube

2.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran / 4 h / Schlenk technique; Glovebox; Cooling

2.2: 10 h / Schlenk technique; Glovebox; Cooling

3.1: hydrogenchloride / water; methanol / 2 h / Reflux

4.1: toluene-4-sulfonic acid / methanol

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; water; 1.3: |Negishi Coupling;
DOI:10.1021/ja4004816