2-mesityl-2-p-tolyl-vinyl alcohol

Base Information

• Chemical Name: 2-mesityl-2-p-tolyl-vinyl alcohol
• CAS No.: 101742-91-0
• Molecular Formula: C₁₈H₂₀O
• Molecular Weight: 252.356
• Mol file: 101742-91-0.mol

Synonyms:

Chemical Property of 2-mesityl-2-p-tolyl-vinyl alcohol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-mesityl-2-p-tolyl-vinyl alcohol

There total 6 articles about 2-mesityl-2-p-tolyl-vinyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

mesityl-p-tolyl ketene (101789-22-4) → 2-mesityl-2-p-tolyl-vinyl alcohol (101742-91-0,117873-86-6)

Guidance literature:

With tert-butylmagnesium chloride;

DOI:10.1021/ja01565a047

Reference yield:

2,4,6-trimethylmandelic acid (20797-56-2) → 2-mesityl-2-p-tolyl-vinyl alcohol (101742-91-0,117873-86-6)

Guidance literature:

Multi-step reaction with 3 steps

1: SnCl₄

2: pyridine; benzene; SOCl₂

3: tert-butyl magnesium chloride

With pyridine; thionyl chloride; tert-butylmagnesium chloride; tin(IV) chloride; benzene;

DOI:10.1021/ja01565a047

Reference yield:

4-methylmandelic acid (18584-20-8,31284-89-6,58690-84-9,75172-62-2) → 2-mesityl-2-p-tolyl-vinyl alcohol (101742-91-0,117873-86-6)

Guidance literature:

Multi-step reaction with 3 steps

1: SnCl₄

2: pyridine; benzene; SOCl₂

3: tert-butyl magnesium chloride

With pyridine; thionyl chloride; tert-butylmagnesium chloride; tin(IV) chloride; benzene;

DOI:10.1021/ja01565a047

upstream raw materials:

mesityl-p-tolyl ketene

2,4,6-trimethylmandelic acid

4-methylmandelic acid

mesityl-p-tolyl-acetic acid

Downstream raw materials:

benzoic acid-(2-mesityl-2-p-tolyl-vinyl ester)