Ph₃PPdSn(1-methyl-2-mercaptoimidazole)2(OC₆H₄NHCOC₃H₂N₂(CH₃))

Base Information

• Chemical Name: Ph₃PPdSn(1-methyl-2-mercaptoimidazole)2(OC₆H₄NHCOC₃H₂N₂(CH₃))
• CAS No.: 1309465-79-9
• Molecular Formula: C₃₇H₃₄N₇O₂PPdS₂Sn
• Molecular Weight: 928.958
• Mol file: 1309465-79-9.mol

Synonyms:

Chemical Property of Ph₃PPdSn(1-methyl-2-mercaptoimidazole)2(OC₆H₄NHCOC₃H₂N₂(CH₃))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Ph₃PPdSn(1-methyl-2-mercaptoimidazole)2(OC₆H₄NHCOC₃H₂N₂(CH₃))

There total 1 articles about Ph₃PPdSn(1-methyl-2-mercaptoimidazole)2(OC₆H₄NHCOC₃H₂N₂(CH₃)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

HOC6H4NHC(O)CN(CH3)CHCHN (1091604-98-6) + Ph3PPdSnCl2(1-methyl-2-mercaptoimidazole)2 (1309465-71-1) → Ph3PPdSn(1-methyl-2-mercaptoimidazole)2(OC6H4NHCOC3H2N2(CH3)) (1309465-79-9)

Guidance literature:

With NEt₃; In dichloromethane; Sn-Pd compd. and HOC6H4NHCOC3H2N2(CH3) stirred in CH2Cl2, and NEt3 added; EtOH added, CH2Cl2 evapd.; ppt. separated by decantation, washed with EtOH, dried in air; elem. anal.;

DOI:10.1002/anie.201007967

upstream raw materials:

HOC₆H₄NHC(O)CN(CH₃)CHCHN

Ph₃PPdSnCl₂(1-methyl-2-mercaptoimidazole)2