CF₃O₃S^(1-)*C₃₃H₂₅N₂O₂⁽¹⁺⁾

Base Information

Chemical Name:CF₃O₃S^(1-)*C₃₃H₂₅N₂O₂⁽¹⁺⁾
CAS No.:1354694-98-6
Molecular Formula:CF₃O₃S*C₃₃H₂₅N₂O₂
Molecular Weight:630.644
Hs Code.:

CF<sub>3</sub>O<sub>3</sub>S<sup>(1-)</sup>*C<sub>33</sub>H<sub>25</sub>N<sub>2</sub>O<sub>2</sub><sup>(1+)</sup>

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Chemical Property of CF₃O₃S^(1-)*C₃₃H₂₅N₂O₂⁽¹⁺⁾

Chemical Property:

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Technology Process of CF₃O₃S^(1-)*C₃₃H₂₅N₂O₂⁽¹⁺⁾

There total 12 articles about CF₃O₃S^(1-)*C₃₃H₂₅N₂O₂⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7-phenyl-2,3-dihydro-1H-inden-1-one

: 1354694-98-6
CF₃O₃S^(1-)*C₃₃H₂₅N₂O₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

2.1: Amberlyst 15 / hexane / 3 h / 0 - 20 °C / Reflux

3.1: C₃₈H₄₂ClMnN₂O₄; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / -78 °C

3.2: -78 °C

4.1: sodium azide; ammonium chloride / ethanol; water / 2 h / Reflux

5.1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h

6.1: acetic acid / tetrahydrofuran / 16 h / 90 °C

7.1: thionyl chloride / toluene / 16 h / 90 °C

8.1: sodium hydroxide / tetrahydrofuran; ethanol / 3 h / 90 °C

9.1: dichloromethane / 2 h / 20 °C / Darkness

With sodium tetrahydroborate; thionyl chloride; sodium azide; palladium 10% on activated carbon; C₃₈H₄₂ClMnN₂O₄; hydrogen; ammonium chloride; acetic acid; 4-methylmorpholine N-oxide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; toluene;
DOI:10.1039/c1ob06780j

Reference yield:

: 868374-23-6
3-oxo-2,3-dihydro-1H-inden-4-yl trifluoromethanesulfonate

: 1354694-98-6
CF₃O₃S^(1-)*C₃₃H₂₅N₂O₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / Inert atmosphere; Reflux

2.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

3.1: Amberlyst 15 / hexane / 3 h / 0 - 20 °C / Reflux

4.1: C₃₈H₄₂ClMnN₂O₄; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / -78 °C

4.2: -78 °C

5.1: sodium azide; ammonium chloride / ethanol; water / 2 h / Reflux

6.1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h

7.1: acetic acid / tetrahydrofuran / 16 h / 90 °C

8.1: thionyl chloride / toluene / 16 h / 90 °C

9.1: sodium hydroxide / tetrahydrofuran; ethanol / 3 h / 90 °C

10.1: dichloromethane / 2 h / 20 °C / Darkness

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; sodium azide; palladium 10% on activated carbon; C₃₈H₄₂ClMnN₂O₄; hydrogen; sodium carbonate; ammonium chloride; acetic acid; 4-methylmorpholine N-oxide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; toluene;
DOI:10.1039/c1ob06780j

Reference yield:

: 6968-35-0
7-hydroxy-indan-1-one

: 1354694-98-6
CF₃O₃S^(1-)*C₃₃H₂₅N₂O₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 11 steps

1.1: triethylamine / dichloromethane / 24 h / 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / Inert atmosphere; Reflux

3.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

4.1: Amberlyst 15 / hexane / 3 h / 0 - 20 °C / Reflux

5.1: C₃₈H₄₂ClMnN₂O₄; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / -78 °C

5.2: -78 °C

6.1: sodium azide; ammonium chloride / ethanol; water / 2 h / Reflux

7.1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h

8.1: acetic acid / tetrahydrofuran / 16 h / 90 °C

9.1: thionyl chloride / toluene / 16 h / 90 °C

10.1: sodium hydroxide / tetrahydrofuran; ethanol / 3 h / 90 °C

11.1: dichloromethane / 2 h / 20 °C / Darkness

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; sodium azide; palladium 10% on activated carbon; C₃₈H₄₂ClMnN₂O₄; hydrogen; sodium carbonate; ammonium chloride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; toluene;
DOI:10.1039/c1ob06780j