Technology Process of C28H26Cl3N7O4S
There total 7 articles about C28H26Cl3N7O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-Aminobenzonitrile;
With
tetrafluoroboric acid; acetic acid; sodium nitrite;
In
water;
at 0 ℃;
C21H23Cl3N4O4S;
In
water; acetonitrile;
at 20 ℃;
DOI:10.5012/bkcs.2011.32.2.664
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / benzene / 12 h / 150 °C
2.1: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C
3.1: copper(I) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 19 h / 20 °C
4.1: tetrafluoroboric acid; acetic acid; sodium nitrite / water / 0 °C
4.2: 20 °C
With
N-Bromosuccinimide; tetrafluoroboric acid; sodium azide; 2,2'-azobis(isobutyronitrile); copper(I) sulfate pentahydrate; acetic acid; sodium L-ascorbate; sodium nitrite;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; benzene;
DOI:10.5012/bkcs.2011.32.2.664
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: copper(I) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 19 h / 20 °C
2.1: tetrafluoroboric acid; acetic acid; sodium nitrite / water / 0 °C
2.2: 20 °C
With
tetrafluoroboric acid; copper(I) sulfate pentahydrate; acetic acid; sodium L-ascorbate; sodium nitrite;
In
tetrahydrofuran; water;
DOI:10.5012/bkcs.2011.32.2.664
