Phenyl-carbamic acid (R)-1-{(2S,4S)-2,5,12-trihydroxy-4-[(2R,4S,5R,6S)-5-hydroxy-6-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacen-2-yl}-ethyl ester

Base Information

• Chemical Name: Phenyl-carbamic acid (R)-1-{(2S,4S)-2,5,12-trihydroxy-4-[(2R,4S,5R,6S)-5-hydroxy-6-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacen-2-yl}-ethyl ester
• CAS No.: 91576-49-7
• Molecular Formula: C₃₅H₃₃F₃N₂O₁₁
• Molecular Weight: 714.649

Synonyms:

Chemical Property of Phenyl-carbamic acid (R)-1-{(2S,4S)-2,5,12-trihydroxy-4-[(2R,4S,5R,6S)-5-hydroxy-6-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacen-2-yl}-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Useful:

Technology Process of Phenyl-carbamic acid (R)-1-{(2S,4S)-2,5,12-trihydroxy-4-[(2R,4S,5R,6S)-5-hydroxy-6-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacen-2-yl}-ethyl ester

There total 11 articles about Phenyl-carbamic acid (R)-1-{(2S,4S)-2,5,12-trihydroxy-4-[(2R,4S,5R,6S)-5-hydroxy-6-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacen-2-yl}-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(7S,9S)-7-<(3'-amino-2',3',6'-trideoxy-4'-O-methyl-α-L-lyxohexopyranosyl)oxy>-7,8,9,10-tetrahydro-6,9,11-trihydroxy-9-<<(phenylcarbamoyl)oxy>methyl>-5,12-naphthacenedione hydrochloride (91576-87-3,91605-43-5) → Phenyl-carbamic acid (R)-1-{(2S,4S)-2,5,12-trihydroxy-4-[(2R,4S,5S,6S)-5-hydroxy-6-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacen-2-yl}-ethyl ester (91576-49-7,91605-40-2,91605-45-7)

Guidance literature:

With sodium hydroxide; In methanol; dichloromethane; at 0 ℃; for 1.5h;

DOI:10.1021/jm00171a011

Reference yield:

4-Nitro-benzoic acid (2S,3R,4S,6R)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-6-[(1S,3S)-3,5,12-trihydroxy-6,11-dioxo-3-((S)-1-phenylcarbamoyloxy-ethyl)-1,2,3,4,6,11-hexahydro-naphthacen-1-yloxy]-tetrahydro-pyran-3-yl ester (91576-48-6,91605-39-9,91605-44-6) → Phenyl-carbamic acid (S)-1-{(2S,4S)-2,5,12-trihydroxy-4-[(2R,4S,5R,6S)-5-hydroxy-6-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacen-2-yl}-ethyl ester (91576-49-7,91605-40-2,91605-45-7)

Guidance literature:

With sodium hydroxide; In methanol; dichloromethane; at 0 ℃; for 1.5h;

DOI:10.1021/jm00171a011

Reference yield:

4-Nitro-benzoic acid (2S,3R,4S,6R)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-6-[(1S,3S)-3,5,12-trihydroxy-6,11-dioxo-3-((R)-1-phenylcarbamoyloxy-ethyl)-1,2,3,4,6,11-hexahydro-naphthacen-1-yloxy]-tetrahydro-pyran-3-yl ester (91576-48-6,91605-39-9,91605-44-6) → Phenyl-carbamic acid (R)-1-{(2S,4S)-2,5,12-trihydroxy-4-[(2R,4S,5R,6S)-5-hydroxy-6-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacen-2-yl}-ethyl ester (91576-49-7,91605-40-2,91605-45-7)

Guidance literature:

With sodium hydroxide; In methanol; dichloromethane; at 0 ℃; for 1.5h;

DOI:10.1021/jm00171a011

upstream raw materials:

4-Nitro-benzoic acid (2S,3R,4S,6R)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-6-[(1S,3S)-3,5,12-trihydroxy-6,11-dioxo-3-((S)-1-phenylcarbamoyloxy-ethyl)-1,2,3,4,6,11-hexahydro-naphthacen-1-yloxy]-tetrahydro-pyran-3-yl ester

4-Nitro-benzoic acid (2S,3R,4S)-6-chloro-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yl ester

(7S,9S)-7,8,9,10-tetrahydro-6,7,9,11-tetrahydroxy-9-<1-(S)-<(phenylcarbamoyl)oxy>ethyl>-5,12-naphthacenedione

C₂₈H₂₃BO₈

Downstream raw materials:

(7S,9S)-7-<(3'-amino-2',3',6'-trideoxy-α-L-arabinohexopyranosyl)oxy>-7,8,9,10-tetrahydro-6,9,11-trihydroxy-9-<1-(R)-<(phenylcarbamoyl)oxy>ethyl>-5,12-naphthacenedione

(7S,9S)-7-<(3'-amino-2',3',6'-trideoxy-α-L-lyxohexopyranosyl)oxy>-7,8,9,10-tetrahydro-6,9,11-trihydroxy-9-<1-(R)-<(phenylcarbamoyl)oxy>ethyl>-5,12-naphthacenedione

(7S,9S)-7-<(3'-amino-2',3',6'-trideoxy-α-L-arabinohexopyranosyl)oxy>-7,8,9,10-tetrahydro-6,9,11-trihydroxy-9-<1-(S)-<(phenylcarbamoyl)oxy>ethyl>-5,12-naphthacenedione

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