(S)-2-((S)-2-Amino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-4-methylsulfanyl-butyric acid tert-butyl ester; hydrochloride

Base Information

Chemical Name:(S)-2-((S)-2-Amino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-4-methylsulfanyl-butyric acid tert-butyl ester; hydrochloride
CAS No.:116823-59-7
Molecular Formula:C₂₈H₃₉N₃O₆S*ClH
Molecular Weight:582.161
Hs Code.:

(S)-2-((S)-2-Amino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-4-methylsulfanyl-butyric acid tert-butyl ester; hydrochloride

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Chemical Property of (S)-2-((S)-2-Amino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-4-methylsulfanyl-butyric acid tert-butyl ester; hydrochloride

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Technology Process of (S)-2-((S)-2-Amino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-4-methylsulfanyl-butyric acid tert-butyl ester; hydrochloride

There total 1 articles about (S)-2-((S)-2-Amino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-4-methylsulfanyl-butyric acid tert-butyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 116823-58-6
Nps-Asn(Mbh)-Met-OBu^t

: 116823-59-7
(S)-2-((S)-2-Amino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-4-methylsulfanyl-butyric acid tert-butyl ester; hydrochloride

Guidance literature:: With hydrogenchloride;
DOI:10.1016/S0040-4039(00)80212-9

Reference yield: 90.0%

: 116823-59-7
(S)-2-((S)-2-Amino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-4-methylsulfanyl-butyric acid tert-butyl ester; hydrochloride

: 116823-57-5
(3R,9S,12S,15S,21S,22S)-12-Isobutyl-15,22-dimethyl-9-(2-methylsulfanyl-ethyl)-5,8,11,14,17,20-hexaoxo-21-(2,2,2-trichloro-ethoxycarbonylamino)-1-thia-4,7,10,13,16,19-hexaaza-cyclodocosane-3-carboxylic acid

: 116823-60-0
C₅₆H₈₁Cl₃N₁₀O₁₅S₃

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide;
DOI:10.1016/S0040-4039(00)80212-9

Reference yield:

: 116823-59-7
(S)-2-((S)-2-Amino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-4-methylsulfanyl-butyric acid tert-butyl ester; hydrochloride

: 116823-44-0
C₅₃H₈₀N₁₀O₁₃S₃*ClH

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 1-ethyl-3-(3-dimethylamino-propyl)-carbodiimide, 1-hydroxybenzotriazole

2: 1.) Zn/AcOH; 2.) HCl

With hydrogenchloride; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; zinc;
DOI:10.1016/S0040-4039(00)80212-9