meso-3,4-dimethyl-3,4-bis(4'-diazoniophenyl)hexane ditetrafluoroborate salt

Base Information

Chemical Name:meso-3,4-dimethyl-3,4-bis(4'-diazoniophenyl)hexane ditetrafluoroborate salt
CAS No.:130379-09-8
Molecular Formula:2BF₄*C₂₀H₂₄N₄
Molecular Weight:494.047
Hs Code.:

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Chemical Property of meso-3,4-dimethyl-3,4-bis(4'-diazoniophenyl)hexane ditetrafluoroborate salt

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Technology Process of meso-3,4-dimethyl-3,4-bis(4'-diazoniophenyl)hexane ditetrafluoroborate salt

There total 3 articles about meso-3,4-dimethyl-3,4-bis(4'-diazoniophenyl)hexane ditetrafluoroborate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10192-93-5
3,4-dimethyl-3,4-diphenylhexane

: 130379-09-8
meso-3,4-dimethyl-3,4-bis(4'-diazoniophenyl)hexane ditetrafluoroborate salt

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid / acetic anhydride

2: H₂ / 10percent Pd/C / ethyl acetate / 3040 Torr

3: boron trifluoride etherate, tert-butyl nitrite / tetrahydrofuran; CH₂Cl₂

With tert.-butylnitrite; boron trifluoride diethyl etherate; hydrogen; nitric acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic anhydride; ethyl acetate;
DOI:10.1021/jo00313a021

Reference yield:

: 345651-60-7
meso-3,4-dimethyl-3,4-bis(4'-nitrophenyl)hexane

: 130379-09-8
meso-3,4-dimethyl-3,4-bis(4'-diazoniophenyl)hexane ditetrafluoroborate salt

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethyl acetate / 3040 Torr

2: boron trifluoride etherate, tert-butyl nitrite / tetrahydrofuran; CH₂Cl₂

With tert.-butylnitrite; boron trifluoride diethyl etherate; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/jo00313a021

Reference yield:

: 130379-07-6
meso-3,4-dimethyl-3,4-bis(4'-aminophenyl)hexane

: 130379-09-8
meso-3,4-dimethyl-3,4-bis(4'-diazoniophenyl)hexane ditetrafluoroborate salt

Guidance literature:: With tert.-butylnitrite; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00313a021