C₁₃H₉BrF₂O

Base Information

Chemical Name:C₁₃H₉BrF₂O
CAS No.:1285028-20-7
Molecular Formula:C₁₃H₉BrF₂O
Molecular Weight:299.115
Hs Code.:

C<sub>13</sub>H<sub>9</sub>BrF<sub>2</sub>O

Synonyms:

Suppliers and Price of C₁₃H₉BrF₂O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₉BrF₂O

Chemical Property:

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Technology Process of C₁₃H₉BrF₂O

There total 1 articles about C₁₃H₉BrF₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 461-96-1
3,5-difluorobromobenzene

: 6630-33-7
ortho-bromobenzaldehyde

: 1285028-20-7
C₁₃H₉BrF₂O

Guidance literature:: 3,5-difluorobromobenzene; With magnesium; In tetrahydrofuran; at 20 ℃; for 0.75h; Inert atmosphere; Heating;

ortho-bromobenzaldehyde; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201206971

Reference yield:

: 1285028-20-7
C₁₃H₉BrF₂O

: 951891-77-3
(2-bromophenyl)(3,5-difluorophenyl)methanone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201206971

Reference yield:

: 1285028-20-7
C₁₃H₉BrF₂O

: 1-(2-bromophenyl)-1-(3,5-difluorophenyl)but-3-yn-1-ol

: 1-(2-bromophenyl)-1-(3,5-difluorophenyl)but-3-yn-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: Walphos-8; sodium t-butanolate; silver fluoride / tert-butyl alcohol; tert-butyl methyl ether / 0.08 h / 20 °C / Inert atmosphere

2.2: 6 h / -20 °C / Inert atmosphere

With Walphos-8; silver fluoride; pyridinium chlorochromate; sodium t-butanolate; In dichloromethane; tert-butyl methyl ether; tert-butyl alcohol;
DOI:10.1002/anie.201206971