C₄₆H₈₀NO₁₅PSi

Base Information

Chemical Name:C₄₆H₈₀NO₁₅PSi
CAS No.:136358-62-8
Molecular Formula:C₄₆H₈₀NO₁₅PSi
Molecular Weight:946.198
Hs Code.:

C<sub>46</sub>H<sub>80</sub>NO<sub>15</sub>PSi

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₆H₈₀NO₁₅PSi

Chemical Property:

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Technology Process of C₄₆H₈₀NO₁₅PSi

There total 12 articles about C₄₆H₈₀NO₁₅PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 136358-62-8,136391-41-8
C₄₆H₈₀NO₁₅PSi

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / 2,6-lutidine / CH₂Cl₂ / 0.25 h / -78 - 20 °C

2: 60.4 percent / dihydroquinidine acetate, OsO₄ / toluene / 5 h

3: 96 percent / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 2 h

4: 80 percent / 4A molecular sieves, camphorsulfonic acid / benzene; tetrahydrofuran / 2 h / Ambient temperature

5: 95 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.33 h

6: 90.8 percent / aq. LiOH / tetrahydrofuran; methanol / 2 h / -15 - -10 °C

7: (benzotriazolyl-1-oxy)tris(dimethylamino)phosphonium hexafluorophosphate (BOP)

With 2,6-dimethylpyridine; lithium hydroxide; osmium(VIII) oxide; hydroquinidine acetate; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; dicyclohexyl-carbodiimide; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; benzene;

Reference yield:

: 136358-53-7,136358-54-8
<2R,S,3R,5S,6S,6(1S,2S)>-2-hydroxy-6-<2-(benzyloxy)-1-methoxy-3-methylbutyl>-5-methoxy-3-methyltetrahydropyran

: 136358-62-8,136391-41-8
C₄₆H₈₀NO₁₅PSi

Guidance literature:: Multi-step reaction with 8 steps

1: 73.5 percent / acetonitrile / 72 h / Heating

2: 93 percent / 2,6-lutidine / CH₂Cl₂ / 0.25 h / -78 - 20 °C

3: 60.4 percent / dihydroquinidine acetate, OsO₄ / toluene / 5 h

4: 96 percent / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 2 h

5: 80 percent / 4A molecular sieves, camphorsulfonic acid / benzene; tetrahydrofuran / 2 h / Ambient temperature

6: 95 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.33 h

7: 90.8 percent / aq. LiOH / tetrahydrofuran; methanol / 2 h / -15 - -10 °C

8: (benzotriazolyl-1-oxy)tris(dimethylamino)phosphonium hexafluorophosphate (BOP)

With 2,6-dimethylpyridine; lithium hydroxide; osmium(VIII) oxide; hydroquinidine acetate; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; dicyclohexyl-carbodiimide; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; acetonitrile; benzene;

Reference yield:

: 136358-37-7
(2E,6S,7S,8R,9S)-7-hydroxy-6,8-dimethoxy-4,10-dimethyl-9-(phenylmethoxy)-2-undecenoic acid methyl ester

: 136358-62-8,136391-41-8
C₄₆H₈₀NO₁₅PSi

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / 2,6-lutidine / CH₂Cl₂ / 0.25 h / -78 - 20 °C

2: 60.4 percent / dihydroquinidine acetate, OsO₄ / toluene / 5 h

3: 96 percent / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 2 h

4: 80 percent / 4A molecular sieves, camphorsulfonic acid / benzene; tetrahydrofuran / 2 h / Ambient temperature

5: 95 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.33 h

6: 90.8 percent / aq. LiOH / tetrahydrofuran; methanol / 2 h / -15 - -10 °C

7: (benzotriazolyl-1-oxy)tris(dimethylamino)phosphonium hexafluorophosphate (BOP)

With 2,6-dimethylpyridine; lithium hydroxide; osmium(VIII) oxide; hydroquinidine acetate; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; dicyclohexyl-carbodiimide; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; benzene;