C₅₈H₇₆N₂O₁₉

Base Information

Chemical Name:C₅₈H₇₆N₂O₁₉
CAS No.:81629-59-6
Molecular Formula:C₅₈H₇₆N₂O₁₉
Molecular Weight:1105.24
Hs Code.:

C<sub>58</sub>H<sub>76</sub>N<sub>2</sub>O<sub>19</sub>

Synonyms:

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Chemical Property of C₅₈H₇₆N₂O₁₉

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Technology Process of C₅₈H₇₆N₂O₁₉

There total 12 articles about C₅₈H₇₆N₂O₁₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79957-36-1,81629-37-0
benzyl 2-acetamido-4,6-di-O-acetyl-2-deoxy-3-O--α-D-glucopyranoside

: 81629-59-6
C₅₈H₇₆N₂O₁₉

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / hydrogen / 10percent Pd/C / methanol; H₂O; acetic acid / 6.5 h / 30 - 35 °C

2: acetyl chloride / 1,2-dichloro-ethane / 22 h / Ambient temperature

3: acetic acid / 1 h / Ambient temperature

4: 94 percent / ferric chloride / CH₂Cl₂ / 1.5 h / Ambient temperature

5: 82 percent / toluene-p-sulfonic acid monohydrate / 1,2-dichloro-ethane / 30 h / 60 °C

6: 91 percent / pyridine / 4 h / Ambient temperature

7: 1.) 0.1 M potassium hydroxide, 2.) Amberlite IR-120 (H+) / 1.) 1,4-dioxane, 5 min., room temp.

With pyridine; potassium hydroxide; Amberlite IR-120 (H+); hydrogen; iron(III) chloride; toluene-4-sulfonic acid; acetyl chloride; palladium on activated charcoal; In methanol; dichloromethane; water; acetic acid; 1,2-dichloro-ethane;
DOI:10.1016/S0008-6215(00)81038-1

Reference yield:

: 1961-72-4,3422-31-9
3-hydroxytetradecanoic acid

: 81629-59-6
C₅₈H₇₆N₂O₁₉

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) N-hydroxysuccinimide, dicyclohexylcarbodiimide / 1.) 1,4-dioxane, 1 h., room temp., 2.) room temp., 1,4-dioxane

2: pyridine

3: 70percent aqueous acetic acid / 1 h / 40 - 45 °C

4: 82 percent / toluene-p-sulfonic acid monohydrate / 1,2-dichloro-ethane / 30 h / 60 °C

5: 91 percent / pyridine / 4 h / Ambient temperature

6: 1.) 0.1 M potassium hydroxide, 2.) Amberlite IR-120 (H+) / 1.) 1,4-dioxane, 5 min., room temp.

With pyridine; potassium hydroxide; 1-hydroxy-pyrrolidine-2,5-dione; Amberlite IR-120 (H+); toluene-4-sulfonic acid; acetic acid; dicyclohexyl-carbodiimide; In 1,2-dichloro-ethane;
DOI:10.1016/S0008-6215(00)81038-1

Reference yield:

: 66026-11-7
O-phenylmethyl 2-amino-2-deoxy-4,6-O-(1-methylethylidene)-α-D-glucopyranoside

: 81629-59-6
C₅₈H₇₆N₂O₁₉

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) N-hydroxysuccinimide, dicyclohexylcarbodiimide / 1.) 1,4-dioxane, 1 h., room temp., 2.) room temp., 1,4-dioxane

2: pyridine

3: 70percent aqueous acetic acid / 1 h / 40 - 45 °C

4: 82 percent / toluene-p-sulfonic acid monohydrate / 1,2-dichloro-ethane / 30 h / 60 °C

5: 91 percent / pyridine / 4 h / Ambient temperature

6: 1.) 0.1 M potassium hydroxide, 2.) Amberlite IR-120 (H+) / 1.) 1,4-dioxane, 5 min., room temp.

With pyridine; potassium hydroxide; 1-hydroxy-pyrrolidine-2,5-dione; Amberlite IR-120 (H+); toluene-4-sulfonic acid; acetic acid; dicyclohexyl-carbodiimide; In 1,2-dichloro-ethane;
DOI:10.1016/S0008-6215(00)81038-1