Carbonic acid 4-[{4-[{4-[allyl-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl ester methyl ester

Base Information

• Chemical Name: Carbonic acid 4-[{4-[{4-[allyl-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl ester methyl ester
• CAS No.: 1027533-10-3
• Molecular Formula: C₄₁H₄₇N₃O₉S₃
• Molecular Weight: 822.037

Synonyms:

Chemical Property of Carbonic acid 4-[{4-[{4-[allyl-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl ester methyl ester

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of Carbonic acid 4-[{4-[{4-[allyl-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl ester methyl ester

There total 5 articles about Carbonic acid 4-[{4-[{4-[allyl-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-oxabicyclo[3.1.0]hex-2-ene (7129-41-1) → Carbonic acid 4-[{4-[{4-[allyl-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl ester methyl ester (1027533-10-3)

Guidance literature:

Multi-step reaction with 5 steps

1: 76 percent / Pd₂dba3-CHCl₃, dppe, BSA / tetrahydrofuran / 2 h / 0 °C

2: 100 percent / pyridine / CH₂Cl₂ / Ambient temperature

3: 79 percent / Pd(PPh₃)4, dppe / tetrahydrofuran

4: Pd₂dba3-CHCl₃, dppe, BSA / tetrahydrofuran / 2 h / 0 °C

5: pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; benzenesulfonamide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jo972279g

Reference yield:

C22H26N2O4S2 → Carbonic acid 4-[{4-[{4-[allyl-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl ester methyl ester (1027533-10-3)

Guidance literature:

Multi-step reaction with 5 steps

1: 76 percent / Pd₂dba3-CHCl₃, dppe, BSA / tetrahydrofuran / 2 h / 0 °C

2: 100 percent / pyridine / CH₂Cl₂ / Ambient temperature

3: 79 percent / Pd(PPh₃)4, dppe / tetrahydrofuran

4: Pd₂dba3-CHCl₃, dppe, BSA / tetrahydrofuran / 2 h / 0 °C

5: pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; benzenesulfonamide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jo972279g

Reference yield:

C27H32N2O5S2 (208249-58-5) → Carbonic acid 4-[{4-[{4-[allyl-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl}-(toluene-4-sulfonyl)-amino]-cyclopent-2-enyl ester methyl ester (1027533-10-3)

Guidance literature:

Multi-step reaction with 4 steps

1: 100 percent / pyridine / CH₂Cl₂ / Ambient temperature

2: 79 percent / Pd(PPh₃)4, dppe / tetrahydrofuran

3: Pd₂dba3-CHCl₃, dppe, BSA / tetrahydrofuran / 2 h / 0 °C

4: pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; benzenesulfonamide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jo972279g

upstream raw materials:

methyl chloroformate

6-oxabicyclo[3.1.0]hex-2-ene

C₂₇H₃₂N₂O₅S₂

C₃₄H₃₉N₃O₆S₃

Downstream raw materials:

C₄₉H₅₆N₄O₈S₄

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