benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-<(tert-butoxycarbonyl)amino>-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Base Information

Chemical Name:benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-<(tert-butoxycarbonyl)amino>-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate
CAS No.:137845-78-4
Molecular Formula:C₃₇H₄₆N₄O₁₁
Molecular Weight:722.792
Hs Code.:

benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-<(tert-butoxycarbonyl)amino>-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Synonyms:

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Chemical Property of benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-<(tert-butoxycarbonyl)amino>-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Chemical Property:

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Technology Process of benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-<(tert-butoxycarbonyl)amino>-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

There total 5 articles about benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-<(tert-butoxycarbonyl)amino>-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₂N₂O₉

: 137845-78-4,137845-79-5
benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-<(tert-butoxycarbonyl)amino>-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 1 h / 0 °C

2: tetrahydrofuran / 0.25 h / 0 °C / Irradiation

3: Bu3SnH, α,α'-azoisobutyronitrile (AIBN) / benzene / 3 h / Heating

4: (CF₃CO₂)2IC₆H₅, pyridine / dimethylformamide; H₂O / 2.5 h / Ambient temperature

5: Et₃N / dimethylformamide / 2 h / Ambient temperature

With pyridine; azobisisobutyronitrile; tri-n-butyl-tin hydride; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00079a007

Reference yield:

: 119750-94-6
(3aS,4S,6R,6aR)-6-(2,4-Dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid 2-thioxo-2H-pyridin-1-yl ester

: 137845-78-4,137845-79-5
benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-<(tert-butoxycarbonyl)amino>-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 0.25 h / 0 °C / Irradiation

2: Bu3SnH, α,α'-azoisobutyronitrile (AIBN) / benzene / 3 h / Heating

3: (CF₃CO₂)2IC₆H₅, pyridine / dimethylformamide; H₂O / 2.5 h / Ambient temperature

4: Et₃N / dimethylformamide / 2 h / Ambient temperature

With pyridine; azobisisobutyronitrile; tri-n-butyl-tin hydride; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00079a007

Reference yield:

: 137845-76-2,137845-77-3
benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-carbamoyl-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

: 137845-78-4,137845-79-5
benzyl 1'-uracil-1-yl-9'-<(benzyloxycarbonyl)amino>-6'(R or S)-<(tert-butoxycarbonyl)amino>-1',5',6',7',8',9'-hexadeoxy-2',3'-O-isopropylidene-β-D-ribo-1',4'-decafuranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: (CF₃CO₂)2IC₆H₅, pyridine / dimethylformamide; H₂O / 2.5 h / Ambient temperature

2: Et₃N / dimethylformamide / 2 h / Ambient temperature

With pyridine; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm00079a007