anti-5--3-phenyl-4,5-dihydroisoxazole

Base Information

Chemical Name:anti-5--3-phenyl-4,5-dihydroisoxazole
CAS No.:138587-65-2
Molecular Formula:C₁₆H₂₁NO₂
Molecular Weight:259.348
Hs Code.:

anti-5-<cyclohexyl(hydroxy)methyl>-3-phenyl-4,5-dihydroisoxazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of anti-5--3-phenyl-4,5-dihydroisoxazole

Chemical Property:

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Technology Process of anti-5--3-phenyl-4,5-dihydroisoxazole

There total 8 articles about anti-5--3-phenyl-4,5-dihydroisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.5%

: 138587-58-3
5-cyclohexylcarbonyl-3-phenyl-4,5-dihydroisoxazole

: 138587-65-2,138587-67-4
syn-5--3-phenyl-4,5-dihydroisoxazole

Guidance literature:: With L-Selectride; In tetrahydrofuran; at -78 ℃; for 8h;
DOI:10.1039/P19910002613

Reference yield:

: 698-16-8
benzohydroximoyl chloride

: 138587-65-2,138587-67-4
syn-5--3-phenyl-4,5-dihydroisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NEt₃ / benzene / 12 h

2: 1) (COCl)2, DMSO, NEt₃ / 1) THF, -78 to -35 deg C, 2) THF, -78 deg C

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In benzene;
DOI:10.1039/P19910002613

Reference yield:

: 2177-34-6
1-cyclohexylprop-2-en-1-one

: 138587-65-2,138587-67-4
syn-5--3-phenyl-4,5-dihydroisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NEt₃ / diethyl ether / 6 h / 25 °C

2: 79.5 percent / L-Selectride / tetrahydrofuran / 8 h / -78 °C

With L-Selectride; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1039/P19910002613