(4-benzyloxy-3-nitro-phenyl)-arsonic acid

Base Information

• Chemical Name: (4-benzyloxy-3-nitro-phenyl)-arsonic acid
• CAS No.: 873985-17-2
• Molecular Formula: C₁₃H₁₂AsNO₆
• Molecular Weight: 353.163
• Mol file: 873985-17-2.mol

Synonyms:

Chemical Property of (4-benzyloxy-3-nitro-phenyl)-arsonic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (4-benzyloxy-3-nitro-phenyl)-arsonic acid

There total 1 articles about (4-benzyloxy-3-nitro-phenyl)-arsonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

roxarsone (121-19-7) + benzyl chloride (100-44-7) → (4-benzyloxy-3-nitro-phenyl)-arsonic acid (873985-17-2)

Guidance literature:

With sodium hydroxide;

DOI:10.1039/jr9310002473 DOI:10.1021/jo01170a019

Reference yield:

(4-benzyloxy-3-nitro-phenyl)-arsonic acid (873985-17-2) → (3-amino-4-benzyloxy-phenyl)-arsonic acid (741258-79-7)

Guidance literature:

With sodium hydroxide; nickel; Hydrogenation;

DOI:10.1021/jo01170a019

Reference yield:

(4-benzyloxy-3-nitro-phenyl)-arsonic acid (873985-17-2) → 5-arsenoso-2-benzyloxy-aniline

Guidance literature:

Multi-step reaction with 2 steps

1: Raney nickel; aqueous methanol. NaOH-solution / Hydrogenation

2: potassium iodide; aqueous hydrochloric acid; sulfur dioxide

With hydrogenchloride; sodium hydroxide; sulfur dioxide; nickel; potassium iodide;

DOI:10.1021/jo01170a019

upstream raw materials:

roxarsone

benzyl chloride

Downstream raw materials:

(3-amino-4-benzyloxy-phenyl)-arsonic acid