benzo[j]fluoranthen-3-ol

Base Information

Chemical Name:benzo[j]fluoranthen-3-ol
CAS No.:106521-01-1
Molecular Formula:C₂₀H₁₂O
Molecular Weight:268.315
Hs Code.:

Synonyms:

Suppliers and Price of benzo[j]fluoranthen-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzo[j]fluoranthen-3-ol

Chemical Property:

Vapor Pressure:9.85E-12mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of benzo[j]fluoranthen-3-ol

There total 12 articles about benzo[j]fluoranthen-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 106521-00-0
4-methoxybenzofluoranthene

: 106521-01-1
4-hydroxybenzofluoranthene

Guidance literature:: With boron tribromide; In dichloromethane; 1.) -78 deg C, 1 h, 2.) RT, 2 h;
DOI:10.1021/jo00381a025

Reference yield:

: 6235-04-7
9-methoxy-11H-benzo fluorene

: 106521-01-1
4-hydroxybenzofluoranthene

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) n-BuLi / 1.) ether, hexane, -30 deg C, 1 h, 2.) ether, hexane, from -30 deg C to RT

2: 69 percent / conc,. H₂SO₄ / benzene / 20 h / Heating

3: 96 percent / 10 N NaOH / pyridine / 3 h / Ambient temperature

4: 97 percent / 10 N NaOH / ethanol / 17 h / Heating

5: 70 percent / methanesulfonic acid / 19 h / Ambient temperature

6: NaBH₄ / methanol / 0.67 h / Ambient temperature

7: p-toluenesulfonic acid / benzene / 2 h / Heating

8: 100 percent / 1-methylnaphthalene / benzene / 7 h / Heating

9: 96 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 1 h, 2.) RT, 2 h

With sodium hydroxide; sodium tetrahydroborate; n-butyllithium; methanesulfonic acid; sulfuric acid; boron tribromide; toluene-4-sulfonic acid; 1-Methylnaphthalene; In pyridine; methanol; ethanol; dichloromethane; benzene;
DOI:10.1021/jo00381a025

Reference yield:

: 106542-96-5
phenyl 2-methoxy-1-naphthoate

: 106521-01-1
4-hydroxybenzofluoranthene

Guidance literature:: Multi-step reaction with 12 steps

1: 68 percent / diethyl ether; benzene / 1.) reflux, 3 h, 2.) RT, overnight

2: 100 percent / methanesulfonic acid / 1.5 h / Ambient temperature

3: 59 percent / zinc amalgam, conc. HCl / toluene; acetic acid / 27 h / Heating

4: 1.) n-BuLi / 1.) ether, hexane, -30 deg C, 1 h, 2.) ether, hexane, from -30 deg C to RT

5: 69 percent / conc,. H₂SO₄ / benzene / 20 h / Heating

6: 96 percent / 10 N NaOH / pyridine / 3 h / Ambient temperature

7: 97 percent / 10 N NaOH / ethanol / 17 h / Heating

8: 70 percent / methanesulfonic acid / 19 h / Ambient temperature

9: NaBH₄ / methanol / 0.67 h / Ambient temperature

10: p-toluenesulfonic acid / benzene / 2 h / Heating

11: 100 percent / 1-methylnaphthalene / benzene / 7 h / Heating

12: 96 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 1 h, 2.) RT, 2 h

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; amalgamated zinc; n-butyllithium; methanesulfonic acid; sulfuric acid; boron tribromide; toluene-4-sulfonic acid; 1-Methylnaphthalene; In pyridine; methanol; diethyl ether; ethanol; dichloromethane; acetic acid; toluene; benzene;
DOI:10.1021/jo00381a025