1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-N-<2-methyl-3',5'-di-O-acetyl-D-ribofurano<1',2':4,5>1,3-dioxolan-2-yl>carboxamide

Base Information

Chemical Name:1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-N-<2-methyl-3',5'-di-O-acetyl-D-ribofurano<1',2':4,5>1,3-dioxolan-2-yl>carboxamide
CAS No.:93512-86-8
Molecular Formula:C₃₃H₃₈N₄O₁₈
Molecular Weight:778.681
Hs Code.:

1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-N-<2-methyl-3',5'-di-O-acetyl-D-ribofurano<1',2':4,5>1,3-dioxolan-2-yl>carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-N-<2-methyl-3',5'-di-O-acetyl-D-ribofurano<1',2':4,5>1,3-dioxolan-2-yl>carboxamide

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Technology Process of 1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-N-<2-methyl-3',5'-di-O-acetyl-D-ribofurano<1',2':4,5>1,3-dioxolan-2-yl>carboxamide

There total 3 articles about 1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-N-<2-methyl-3',5'-di-O-acetyl-D-ribofurano<1',2':4,5>1,3-dioxolan-2-yl>carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53402-29-2
2,3,5-tri-O-acetyl-β-D-ribofuranosyl chloride

: 93512-86-8
1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-N-<2-methyl-3',5'-di-O-acetyl-D-ribofurano<1',2':4,5>1,3-dioxolan-2-yl>carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1,3,3-tetramethylurea / CH₂Cl₂; nitromethane / -20 °C

2: 2) NaHCO₃ / 1) CH₂Cl₂, CH₃NO₂, benzene, room temp.; 2) water, 0 deg C

With sodium hydrogencarbonate; tetramethylurea; In nitromethane; dichloromethane;
DOI:10.1002/jhet.5570210342

Reference yield:

: 13035-61-5
1,2,3,5-tetraacetylribose

: 93512-86-8
1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-N-<2-methyl-3',5'-di-O-acetyl-D-ribofurano<1',2':4,5>1,3-dioxolan-2-yl>carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: HCl(g) / CH₂Cl₂ / 2.5 h / 0 °C

2: 1,1,3,3-tetramethylurea / CH₂Cl₂; nitromethane / -20 °C

3: 2) NaHCO₃ / 1) CH₂Cl₂, CH₃NO₂, benzene, room temp.; 2) water, 0 deg C

With hydrogenchloride; sodium hydrogencarbonate; tetramethylurea; In nitromethane; dichloromethane;
DOI:10.1002/jhet.5570210342

Reference yield:

: 2,3,5-tri-O-acetyl-β-D-ribofuranosyl triflate

: 85240-41-1
C₂₃H₃₆N₄O₄Sn

: 85240-62-6
1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-carboxamide

: 93512-86-8
1-(4-nitrobenzyl)-4-(2,3,5-tri-O-acetyl-β-D-ribofuranosyloxy)-1H-imidazole-5-N-<2-methyl-3',5'-di-O-acetyl-D-ribofurano<1',2':4,5>1,3-dioxolan-2-yl>carboxamide

Guidance literature:: With sodium hydrogencarbonate; Yield given. Multistep reaction. Yields of byproduct given; 1) CH₂Cl₂, CH₃NO₂, benzene, room temp.; 2) water, 0 deg C;
DOI:10.1002/jhet.5570210342