Methyl l-2(R)-Methyl-6-p-toluenesulfonyloxyhexanoate

Base Information

Chemical Name:Methyl l-2(R)-Methyl-6-p-toluenesulfonyloxyhexanoate
CAS No.:75584-09-7
Molecular Formula:C₁₅H₂₂O₅S
Molecular Weight:314.403
Hs Code.:

Synonyms:

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Chemical Property of Methyl l-2(R)-Methyl-6-p-toluenesulfonyloxyhexanoate

Chemical Property:

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Technology Process of Methyl l-2(R)-Methyl-6-p-toluenesulfonyloxyhexanoate

There total 6 articles about Methyl l-2(R)-Methyl-6-p-toluenesulfonyloxyhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22629-98-7
Diethyl 4-Methoxybutylmalonate

: 75584-09-7
Methyl l-2(R)-Methyl-6-p-toluenesulfonyloxyhexanoate

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) NaOEt / 1.) EtOH, room temp., 20 min, 2.) EtOH, reflux, 2 h

2: KOH / H₂O; ethanol / 2 h / Heating

3: 2 h / 160 °C

4: diethyl ether

5: 261 mg / BBr₃ / CH₂Cl₂ / 1 h / 0 °C

6: 338 mg / pyridine / 3.5 h / Ambient temperature

With potassium hydroxide; sodium ethanolate; boron tribromide; In pyridine; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1248/cpb.28.1422

Reference yield:

: 75584-07-5
Methyl l-2-(R)-Methyl-6-methoxyhexanoate

: 75584-09-7
Methyl l-2(R)-Methyl-6-p-toluenesulfonyloxyhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 261 mg / BBr₃ / CH₂Cl₂ / 1 h / 0 °C

2: 338 mg / pyridine / 3.5 h / Ambient temperature

With boron tribromide; In pyridine; dichloromethane;
DOI:10.1248/cpb.28.1422

Reference yield:

: 2-(4-Methoxy-butyl)-2-methyl-malonic acid

: 75584-09-7
Methyl l-2(R)-Methyl-6-p-toluenesulfonyloxyhexanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 2 h / 160 °C

2: diethyl ether

3: 261 mg / BBr₃ / CH₂Cl₂ / 1 h / 0 °C

4: 338 mg / pyridine / 3.5 h / Ambient temperature

With boron tribromide; In pyridine; diethyl ether; dichloromethane;
DOI:10.1248/cpb.28.1422