2,2,5,5-Tetramethyl-4,4-diphenylhexan

Base Information

• Chemical Name: 2,2,5,5-Tetramethyl-4,4-diphenylhexan
• CAS No.: 104142-13-4
• Molecular Formula: C₂₂H₃₀
• Molecular Weight: 294.48
• Mol file: 104142-13-4.mol

Synonyms:

Chemical Property of 2,2,5,5-Tetramethyl-4,4-diphenylhexan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2,5,5-Tetramethyl-4,4-diphenylhexan

There total 3 articles about 2,2,5,5-Tetramethyl-4,4-diphenylhexan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-diphenyl-3,3-dimethylbutane (57123-34-9) + tert-butylmercury chloride (38442-51-2) → 2,2,5,5-Tetramethyl-4,4-diphenylhexan (104142-13-4)

Guidance literature:

With Diethyl methylmalonate; In dimethyl sulfoxide; at 35 - 40 ℃; for 12h; Yield given; Irradiation;

DOI:10.1039/c39860000632

Reference yield:

1,1-Diphenylethylene (530-48-3) + tert-butylmercury chloride (38442-51-2) → 1,1-diphenyl-3,3-dimethylbutane (57123-34-9) + 2,2,5,5-Tetramethyl-4,4-diphenylhexan (104142-13-4)

Guidance literature:

With potassium tert-butylate; Diethyl methylmalonate; In dimethyl sulfoxide; at 35 - 40 ℃; for 12h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Irradiation;

DOI:10.1039/c39860000632

Reference yield:

1,1-Diphenylethylene (530-48-3) + tert.-butyl lithium (594-19-4) → 2,2,5,5-Tetramethyl-4,4-diphenylhexan (104142-13-4)

Guidance literature:

Multistep reaction; (i) ZnCl₂, Et₂O, (ii) /BRN= 1099062/, (III) aq. HCl;

upstream raw materials:

1,1-Diphenylethylene

tert.-butyl lithium

tert-butylmercury chloride

1,1-diphenyl-3,3-dimethylbutane