C₅₄H₄₆N₆O₂P₂

Base Information

Chemical Name:C₅₄H₄₆N₆O₂P₂
CAS No.:141258-02-8
Molecular Formula:C₅₄H₄₆N₆O₂P₂
Molecular Weight:872.946
Hs Code.:

C<sub>54</sub>H<sub>46</sub>N<sub>6</sub>O<sub>2</sub>P<sub>2</sub>

Synonyms:

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Chemical Property of C₅₄H₄₆N₆O₂P₂

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Technology Process of C₅₄H₄₆N₆O₂P₂

There total 5 articles about C₅₄H₄₆N₆O₂P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40515-19-3
2-azido-1-methyl-4-nitrobenzene

: 141258-02-8
C₅₄H₄₆N₆O₂P₂

Guidance literature:: Multi-step reaction with 5 steps

1: 48 percent / N-bromosuccinimide, benzoyl peroxide / benzene / 4 h / Heating

2: dimethylformamide / 12 h / 80 °C

3: 85percent aqueous hydrazine / ethanol / 3 h / Heating

4: 83 percent / acetic acid / ethanol / 12 h / Ambient temperature

5: 2) sodium borohydride / 1) ether, CH₂Cl₂, r.t., 12 h, 2) CH₂Cl₂, CH₃OH, 0 deg C, 1.5 h

With sodium tetrahydroborate; N-Bromosuccinimide; Perbenzoic acid; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00059a015

Reference yield:

: 146954-06-5
2-azido-4-nitrobenzylamine

: 141258-02-8
C₅₄H₄₆N₆O₂P₂

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / acetic acid / ethanol / 12 h / Ambient temperature

2: 2) sodium borohydride / 1) ether, CH₂Cl₂, r.t., 12 h, 2) CH₂Cl₂, CH₃OH, 0 deg C, 1.5 h

With sodium tetrahydroborate; acetic acid; In ethanol;
DOI:10.1021/jo00059a015

Reference yield:

: 146954-10-1
2-azido-4-nitrobenzyl bromide

: 141258-02-8
C₅₄H₄₆N₆O₂P₂

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylformamide / 12 h / 80 °C

2: 85percent aqueous hydrazine / ethanol / 3 h / Heating

3: 83 percent / acetic acid / ethanol / 12 h / Ambient temperature

4: 2) sodium borohydride / 1) ether, CH₂Cl₂, r.t., 12 h, 2) CH₂Cl₂, CH₃OH, 0 deg C, 1.5 h

With sodium tetrahydroborate; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00059a015