12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-2,2,5,5,14,14-hexaoxid

Base Information

Chemical Name:12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-2,2,5,5,14,14-hexaoxid
CAS No.:77776-25-1
Molecular Formula:C₃₀H₂₈O₆S₃
Molecular Weight:580.747
Hs Code.:

Synonyms:

Suppliers and Price of 12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-2,2,5,5,14,14-hexaoxid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-2,2,5,5,14,14-hexaoxid

Chemical Property:

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Technology Process of 12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-2,2,5,5,14,14-hexaoxid

There total 6 articles about 12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-2,2,5,5,14,14-hexaoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77776-07-9
12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-14,14-dioxid

: 77776-25-1,77843-19-7,344800-39-1
12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-2,2,5,5,14,14-hexaoxid

Guidance literature:: With dihydrogen peroxide; In acetic acid; benzene; at 70 ℃; for 6h; Yield given;

Reference yield:

: 3976-34-9
2,6-dimethyl-1,1′-biphenyl

: 77776-25-1,77843-19-7,344800-39-1
12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-2,2,5,5,14,14-hexaoxid

Guidance literature:: Multi-step reaction with 6 steps

1: 46 percent / N-bromosuccinimide / methyl formate / 2 h / Irradiation

2: thioacetamide, KOH / ethanol; benzene / 4 h / Heating

3: 87 percent / 30percent H₂O₂ / acetic acid / 4 h / 60 °C

4: 72 percent / N-bromosuccinimide / CH₂Cl₂ / 3 h / Irradiation

5: 30 percent / KOH / aq. ethanol; benzene / 10 h / Heating

6: 30percent H₂O₂ / benzene; acetic acid / 6 h / 70 °C

With potassium hydroxide; N-Bromosuccinimide; dihydrogen peroxide; thioacetamide; In ethanol; dichloromethane; Methyl formate; acetic acid; benzene;

Reference yield:

: 77775-96-3
2-bromomethyl-6-methylbiphenyl

: 77776-25-1,77843-19-7,344800-39-1
12,21-Diphenyl-2,5,14-trithia<6.3>metacyclophan-2,2,5,5,14,14-hexaoxid

Guidance literature:: Multi-step reaction with 5 steps

1: thioacetamide, KOH / ethanol; benzene / 4 h / Heating

2: 87 percent / 30percent H₂O₂ / acetic acid / 4 h / 60 °C

3: 72 percent / N-bromosuccinimide / CH₂Cl₂ / 3 h / Irradiation

4: 30 percent / KOH / aq. ethanol; benzene / 10 h / Heating

5: 30percent H₂O₂ / benzene; acetic acid / 6 h / 70 °C

With potassium hydroxide; N-Bromosuccinimide; dihydrogen peroxide; thioacetamide; In ethanol; dichloromethane; acetic acid; benzene;