6-O-[2-azido-4-O-(tert-butyldimethylsilyl)-2-deoxy-3,6-di-O-(p-methoxybenzyl)-α-Dglucopyranosyl]-1-O-allyl-2,3,4,5-tetra-O-(p-methoxybenzyl)-myo-inositol

Base Information

Chemical Name:6-O-[2-azido-4-O-(tert-butyldimethylsilyl)-2-deoxy-3,6-di-O-(p-methoxybenzyl)-α-Dglucopyranosyl]-1-O-allyl-2,3,4,5-tetra-O-(p-methoxybenzyl)-myo-inositol
CAS No.:1227637-08-2
Molecular Formula:C₆₉H₈₇N₃O₁₆Si
Molecular Weight:1242.55
Hs Code.:

6-O-[2-azido-4-O-(tert-butyldimethylsilyl)-2-deoxy-3,6-di-O-(p-methoxybenzyl)-α-Dglucopyranosyl]-1-O-allyl-2,3,4,5-tetra-O-(p-methoxybenzyl)-myo-inositol

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Chemical Property of 6-O-[2-azido-4-O-(tert-butyldimethylsilyl)-2-deoxy-3,6-di-O-(p-methoxybenzyl)-α-Dglucopyranosyl]-1-O-allyl-2,3,4,5-tetra-O-(p-methoxybenzyl)-myo-inositol

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Technology Process of 6-O-[2-azido-4-O-(tert-butyldimethylsilyl)-2-deoxy-3,6-di-O-(p-methoxybenzyl)-α-Dglucopyranosyl]-1-O-allyl-2,3,4,5-tetra-O-(p-methoxybenzyl)-myo-inositol

There total 1 articles about 6-O-[2-azido-4-O-(tert-butyldimethylsilyl)-2-deoxy-3,6-di-O-(p-methoxybenzyl)-α-Dglucopyranosyl]-1-O-allyl-2,3,4,5-tetra-O-(p-methoxybenzyl)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1227637-09-3
C₃₀H₄₁Cl₃N₄O₇Si

: 1227637-01-5
(-)-1-O-allyl-2,3,4,5-tetra-O-(p-methoxybenzyl)-myo-inositol

: C₆₉H₈₇N₃O₁₆Si

: 1227637-08-2
6-O-[2-azido-4-O-(tert-butyldimethylsilyl)-2-deoxy-3,6-di-O-(p-methoxybenzyl)-α-Dglucopyranosyl]-1-O-allyl-2,3,4,5-tetra-O-(p-methoxybenzyl)-myo-inositol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -10 ℃; for 0.166667h; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja1009037

Reference yield:

: 1227637-08-2
6-O-[2-azido-4-O-(tert-butyldimethylsilyl)-2-deoxy-3,6-di-O-(p-methoxybenzyl)-α-Dglucopyranosyl]-1-O-allyl-2,3,4,5-tetra-O-(p-methoxybenzyl)-myo-inositol

: C₆₉H₈₇N₃O₁₆Si

Guidance literature:: With (1,5-cyclooctadiene)[bis(methyldiphenylphosphine)]iridium(I) hexafluorophosphate; hydrogen; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja1009037