5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

Base Information

Chemical Name:5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide
CAS No.:96792-11-9
Molecular Formula:C₂₈H₄₁N₅O₆
Molecular Weight:543.663
Hs Code.:

5(S)-<<N<sup>α</sup>-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

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Technology Process of 5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

There total 4 articles about 5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96792-10-8
5(S)-<ε-(butyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

: 96792-11-9
5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 0.25h; Ambient temperature;
DOI:10.1021/jm00146a015

Reference yield:

: 96792-09-5
5(S)-<ε-(butyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoic acid

: 96792-11-9
5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide / CH₂Cl₂; dimethylformamide / 20 h / Ambient temperature

2: Et₃N / CH₂Cl₂; dimethylformamide / 5 h / Ambient temperature

3: CF₃COOH / CH₂Cl₂ / 0.25 h / Ambient temperature

With triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00146a015

Reference yield:

: 96792-08-4
2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<1(S)-<ε-(benzyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-2-phenylethyl>-1,3-dioxolane

: 96792-11-9
5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) CrO₃, H₂SO₄, 2.) 2N HCl, H₂, 3.) 90percent aq. CF₃COOH, 4.) Et₃N

2: dicyclohexylcarbodiimide / CH₂Cl₂; dimethylformamide / 20 h / Ambient temperature

3: Et₃N / CH₂Cl₂; dimethylformamide / 5 h / Ambient temperature

4: CF₃COOH / CH₂Cl₂ / 0.25 h / Ambient temperature

With chromium(VI) oxide; hydrogenchloride; sulfuric acid; hydrogen; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00146a015