Technology Process of 1-(diazoacetonylidene)-4-tert-butylcyclohexane
There total 5 articles about 1-(diazoacetonylidene)-4-tert-butylcyclohexane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84 percent / 6percent methanolic potassium hydroxide / 12 h / 40 °C
2: 1) sodium methoxide, 2) oxalyl chloride / 1) MeOH, 2) benzene, 0 deg C, 3 h
3: triethylamine / diethyl ether / 0 °C
With
potassium hydroxide; oxalyl dichloride; sodium methylate; triethylamine;
In
diethyl ether;
DOI:10.1021/jo00288a052
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / N,N-dimethylaniline / CHCl3 / 12 h / Heating
2: 64 percent / sodium ethoxide / ethanol / 12 h / 40 °C
3: 84 percent / 6percent methanolic potassium hydroxide / 12 h / 40 °C
4: 1) sodium methoxide, 2) oxalyl chloride / 1) MeOH, 2) benzene, 0 deg C, 3 h
5: triethylamine / diethyl ether / 0 °C
With
potassium hydroxide; oxalyl dichloride; sodium methylate; sodium ethanolate; N,N-dimethyl-aniline; triethylamine;
In
diethyl ether; ethanol; chloroform;
DOI:10.1021/jo00288a052
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1) sodium methoxide, 2) oxalyl chloride / 1) MeOH, 2) benzene, 0 deg C, 3 h
2: triethylamine / diethyl ether / 0 °C
With
oxalyl dichloride; sodium methylate; triethylamine;
In
diethyl ether;
DOI:10.1021/jo00288a052
