adenosine 5'-<4<(E)-2-nitroethenyl>phenyl glutarate>

Base Information

Chemical Name:adenosine 5'-<4<(E)-2-nitroethenyl>phenyl glutarate>
CAS No.:142728-13-0
Molecular Formula:C₂₃H₂₄N₆O₉
Molecular Weight:528.478
Hs Code.:

Synonyms:

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Chemical Property of adenosine 5'-<4<(E)-2-nitroethenyl>phenyl glutarate>

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Technology Process of adenosine 5'-<4<(E)-2-nitroethenyl>phenyl glutarate>

There total 4 articles about adenosine 5'-<4<(E)-2-nitroethenyl>phenyl glutarate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 142728-11-8
2',3'-O-isopropylideneadenosine 5'-[4-((E)-2-nitroethenyl)phenyl glutarate]

: 142728-13-0
adenosine 5'-<4<(E)-2-nitroethenyl>phenyl glutarate>

Guidance literature:: With hydrogenchloride; In acetone; for 22h; Ambient temperature;
DOI:10.1002/hlca.19920750304

Reference yield:

: 22568-49-6
(E)-1-(4-hydroxyphenyl)-2-nitroethene

: 142728-13-0
adenosine 5'-<4<(E)-2-nitroethenyl>phenyl glutarate>

Guidance literature:: Multi-step reaction with 3 steps

1: 4-(dimethylamino)pyridine / CHCl₃ / 26 h / Ambient temperature

2: 1) oxalyl chloride, DMF, 2) 4-(dimethylamino)pyridine / 1) CHCl₃, 2 h, 2) DMF, r.t., 3 h

3: 31 percent / 1N HCl / acetone / 22 h / Ambient temperature

With hydrogenchloride; dmap; oxalyl dichloride; N,N-dimethyl-formamide; In chloroform; acetone;
DOI:10.1002/hlca.19920750304

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 142728-13-0
adenosine 5'-<4<(E)-2-nitroethenyl>phenyl glutarate>

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / aniline / 6 h / 80 °C

2: 4-(dimethylamino)pyridine / CHCl₃ / 26 h / Ambient temperature

3: 1) oxalyl chloride, DMF, 2) 4-(dimethylamino)pyridine / 1) CHCl₃, 2 h, 2) DMF, r.t., 3 h

4: 31 percent / 1N HCl / acetone / 22 h / Ambient temperature

With hydrogenchloride; dmap; oxalyl dichloride; N,N-dimethyl-formamide; aniline; In chloroform; acetone;
DOI:10.1002/hlca.19920750304