C₁₄H₁₃NO

Base Information

• Chemical Name: C₁₄H₁₃NO
• CAS No.: 74717-09-2
• Molecular Formula: C₁₄H₁₃NO
• Molecular Weight: 211.263
• Mol file: 74717-09-2.mol

Synonyms:

Chemical Property of C₁₄H₁₃NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₄H₁₃NO

There total 1 articles about C₁₄H₁₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(chlorocarbonyl)pyridine (14254-57-0) + ethylbenzene (100-41-4,27536-89-6) → C14H13NO (74717-09-2)

Guidance literature:

With aluminum (III) chloride;

DOI:10.3390/molecules16118945

Reference yield:

diethoxyphosphoryl-acetic acid ethyl ester (867-13-0) + C14H13NO (74717-09-2) → C18H19NO2

Guidance literature:

diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; at 0 ℃;

C₁₄H₁₃NO; In tetrahydrofuran; at 20 ℃; for 10h;

DOI:10.3390/molecules16118945

Reference yield:

C14H13NO (74717-09-2) → C16H14ClNO

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0 °C

1.2: 10 h / 20 °C

2.1: methanol; sodium hydroxide / 10 h / 20 °C

3.1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 8 h / 0 °C

With methanol; thionyl chloride; sodium hydride; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; dichloromethane; 1.1: Wittig-Horner reaction;

DOI:10.3390/molecules16118945

upstream raw materials:

4-(chlorocarbonyl)pyridine

ethylbenzene