Technology Process of C11H15(2)H2ClO
There total 9 articles about C11H15(2)H2ClO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 91 percent / H+ / 140 °C
2: KOH, H2O / methanol
3: KI3, NaHCO3 / H2O
4: DBU / toluene / 110 °C
5: DIBAL-D / CH2Cl2 / -78 °C
6: CCl4, PPh3 / acetonitrile
With
tetrachloromethane; potassium hydroxide; potassium triiodide; water; hydrogen cation; diisobutylaluminium deuteride; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine;
In
methanol; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/jo00234a029
- Guidance literature:
-
Multi-step reaction with 5 steps
1: KOH, H2O / methanol
2: KI3, NaHCO3 / H2O
3: DBU / toluene / 110 °C
4: DIBAL-D / CH2Cl2 / -78 °C
5: CCl4, PPh3 / acetonitrile
With
tetrachloromethane; potassium hydroxide; potassium triiodide; water; diisobutylaluminium deuteride; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine;
In
methanol; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/jo00234a029
- Guidance literature:
-
With
tetrachloromethane; triphenylphosphine;
In
acetonitrile;
DOI:10.1021/jo00234a029