(E)-3,4'-dimethoxy-5-6)-β-D-glucopyranosyloxy>stilbene

Base Information

• Chemical Name: (E)-3,4'-dimethoxy-5-6)-β-D-glucopyranosyloxy>stilbene
• CAS No.: 113021-31-1
• Molecular Formula: C₂₈H₃₆O₁₂
• Molecular Weight: 564.587

Synonyms:

Chemical Property of (E)-3,4'-dimethoxy-5-6)-β-D-glucopyranosyloxy>stilbene

Chemical Property:

Purity/Quality:

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Technology Process of (E)-3,4'-dimethoxy-5-6)-β-D-glucopyranosyloxy>stilbene

There total 1 articles about (E)-3,4'-dimethoxy-5-6)-β-D-glucopyranosyloxy>stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 5,4'-trihydroxy-trans-stilbene-3-yl-[α-L-rhamnopyranosyl-(1→6)-β-D-glucopyranoside] → (E)-3,4'-dimethoxy-5-6)-β-D-glucopyranosyloxy>stilbene (113021-31-1) + trans-4',5-dihydroxy-3-methoxystilbene-5-O-[α-L-rhamnopyranosyl-(1->6)]-β-D-glucopyranoside + 4'-methoxy-(E)-resveratrol 3-O-rutinoside

Guidance literature:

In diethyl ether; for 6h;

DOI:10.1016/S0367-326X(01)00295-7

Reference yield:

(E)-3,4'-dimethoxy-5-6)-β-D-glucopyranosyloxy>stilbene (113021-31-1) → 3,4'-dimethoxy-5-hydroxystilbene (58436-29-6)

Guidance literature:

With hydrogenchloride; In methanol; for 9h; Heating;

DOI:10.1016/0031-9422(94)00915-G

Reference yield:

acetic anhydride (108-24-7) + (E)-3,4'-dimethoxy-5-6)-β-D-glucopyranosyloxy>stilbene (113021-31-1) → (E)-3,4'-dimethoxy-5-<2,3,4-tri-O-acetyl-6-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranosyloxy>stilbene (113021-32-2)

Guidance literature:

With pyridine; Ambient temperature;

upstream raw materials:

diazomethane

Downstream raw materials:

(E)-3,4'-dimethoxy-5-<2,3,4-tri-O-acetyl-6-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranosyloxy>stilbene

3,4'-dimethoxy-5-hydroxystilbene

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