C₂₅H₂₆N₂O₂

Base Information

Chemical Name:C₂₅H₂₆N₂O₂
CAS No.:918803-48-2
Molecular Formula:C₂₅H₂₆N₂O₂
Molecular Weight:386.494
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₆N₂O₂

Chemical Property:

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Technology Process of C₂₅H₂₆N₂O₂

There total 5 articles about C₂₅H₂₆N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 918803-45-9
12-(4-methoxy-benzyl)-10-oxo-5,6,7,8,9,10,11,12-octahydro-7,12-diaza-cyclonona[a]indene-11-carboxylic acid tert-butyl ester

: 918803-48-2
C₂₅H₂₆N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 83 percent / hydrochloric acid / ethanol; H₂O / 1 h / 20 °C

2.1: LDA / hexane; tetrahydrofuran / 1 h / -78 °C

2.2: diethyl ether; tetrahydrofuran; hexane / 1 h / -78 °C

3.1: 747 mg / DMAP; DBU; trifluoroacetic anhydride / CH₂Cl₂ / -42 - 20 °C

4.1: 53 percent / anhydrous AlCl₃ / benzene / 4 h / 20 °C

With hydrogenchloride; dmap; aluminium trichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; benzene; 1.1: Mannich reaction / 2.2: aldol condensation;
DOI:10.1021/jo061724h

Reference yield:

: 918803-44-8
11-(4-methoxy-benzyl)-1-oxo-2,3,6,11-tetrahydro-1H,5H-indolizino[8,7-b]indole-11b-carboxylic acid tert-butyl ester

: 918803-48-2
C₂₅H₂₆N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 86 percent / SmI₂ / tetrahydrofuran / 3 h / 20 °C

2.1: 83 percent / hydrochloric acid / ethanol; H₂O / 1 h / 20 °C

3.1: LDA / hexane; tetrahydrofuran / 1 h / -78 °C

3.2: diethyl ether; tetrahydrofuran; hexane / 1 h / -78 °C

4.1: 747 mg / DMAP; DBU; trifluoroacetic anhydride / CH₂Cl₂ / -42 - 20 °C

5.1: 53 percent / anhydrous AlCl₃ / benzene / 4 h / 20 °C

With hydrogenchloride; dmap; aluminium trichloride; samarium diiodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; benzene; 2.1: Mannich reaction / 3.2: aldol condensation;
DOI:10.1021/jo061724h

Reference yield:

: 918803-46-0
C₂₈H₃₂N₂O₄

: 918803-48-2
C₂₅H₂₆N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: diethyl ether; tetrahydrofuran; hexane / 1 h / -78 °C

2.1: 747 mg / DMAP; DBU; trifluoroacetic anhydride / CH₂Cl₂ / -42 - 20 °C

3.1: 53 percent / anhydrous AlCl₃ / benzene / 4 h / 20 °C

With dmap; aluminium trichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; benzene; 1.2: aldol condensation;
DOI:10.1021/jo061724h