Technology Process of C17H20O2
There total 3 articles about C17H20O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
Molecular sieve;
DOI:10.1021/ja309978c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,5-hexadienerhodium(I)-chloride dimer; tetra(n-butyl)ammonium hydrogensulfate; hydrogen / hexane; diethyl ether / 36 h / 20 °C / 25858.1 Torr / pH 7.6 / Inert atmosphere
2: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve
With
tetrapropylammonium perruthennate; 1,5-hexadienerhodium(I)-chloride dimer; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; 4-methylmorpholine N-oxide;
In
diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja309978c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-DTBM-SEGPHOS / 1,4-dioxane / 48 h / 133 °C / Inert atmosphere
2: 1,5-hexadienerhodium(I)-chloride dimer; tetra(n-butyl)ammonium hydrogensulfate; hydrogen / hexane; diethyl ether / 36 h / 20 °C / 25858.1 Torr / pH 7.6 / Inert atmosphere
3: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve
With
chloro(1,5-cyclooctadiene)rhodium(I) dimer; tetrapropylammonium perruthennate; 1,5-hexadienerhodium(I)-chloride dimer; (R)-DTBM-SEGPHOS; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; 4-methylmorpholine N-oxide;
In
1,4-dioxane; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja309978c
