Benzeneethanol, 2-iodo-3-nitro-, 1-acetate

Base Information

Chemical Name:Benzeneethanol, 2-iodo-3-nitro-, 1-acetate
CAS No.:95067-36-0
Molecular Formula:C₁₀H₁₀INO₄
Molecular Weight:335.098
Hs Code.:
DSSTox Substance ID:DTXSID901266032

Synonyms:Benzeneethanol, 2-iodo-3-nitro-, 1-acetate;DTXSID901266032;95067-36-0

Suppliers and Price of Benzeneethanol, 2-iodo-3-nitro-, 1-acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzeneethanol, 2-iodo-3-nitro-, 1-acetate

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:334.96546
Heavy Atom Count:16
Complexity:266

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)OCCC1=C(C(=CC=C1)[N+](=O)[O-])I

Technology Process of Benzeneethanol, 2-iodo-3-nitro-, 1-acetate

There total 3 articles about Benzeneethanol, 2-iodo-3-nitro-, 1-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95067-33-7
2-(2-acetamidophenyl)ethyl acetate

: 95067-36-0
2-(2-iodo-3-nitrophenyl)ethyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / 60percent aq. HNO₃, Ac₂O / acetic acid / 2 h / 5 °C

2: 99 percent / aq. KOH / 0.5 h / 80 °C

3: 1.) NaNO₂, HCl, urea, 2.) HBF₄, KI, I₂

With hydrogenchloride; potassium hydroxide; tetrafluoroboric acid; iodine; nitric acid; acetic anhydride; urea; potassium iodide; sodium nitrite; In acetic acid;

Reference yield:

: 95067-34-8
2-(2-acetamido-3-nitrophenyl)ethyl acetate

: 95067-36-0
2-(2-iodo-3-nitrophenyl)ethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / aq. KOH / 0.5 h / 80 °C

2: 1.) NaNO₂, HCl, urea, 2.) HBF₄, KI, I₂

With hydrogenchloride; potassium hydroxide; tetrafluoroboric acid; iodine; urea; potassium iodide; sodium nitrite;

Reference yield:

: 108-24-7
acetic anhydride

: 95067-35-9
2-(2-amino-3-nitrophenyl)ethanol

: 95067-36-0
2-(2-iodo-3-nitrophenyl)ethyl acetate

Guidance literature:: With hydrogenchloride; tetrafluoroboric acid; iodine; urea; potassium iodide; sodium nitrite; Yield given. Multistep reaction;