Technology Process of C44H49F5N8O7S2
There total 10 articles about C44H49F5N8O7S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
2: 1.) HCl, 2.) HCl / 1.) CHCl3, 2.) reflux, 3 d
3: NaOH / dioxane; H2O / 1 h / Ambient temperature
4: diphenyl phosphorazidate, Et3N / dioxane / 14 h / 0 °C
5: 1.) NaOH, 2.) DCCD / 1.) dioxane, H2O, room temperature, 1 h, 2.) dioxane, from 0 grad C to room temperature
6: trifluoroacetic acid / 1 h / 0 °C
With
hydrogenchloride; sodium hydroxide; diphenyl phosphoryl azide; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
1,4-dioxane; water;
DOI:10.1016/S0040-4039(00)83967-2
- Guidance literature:
-
Multi-step reaction with 6 steps
2: 1.) HCl, 2.) HCl / 1.) CHCl3, 2.) reflux, 3 d
3: NaOH / dioxane; H2O / 1 h / Ambient temperature
4: diphenyl phosphorazidate, Et3N / dioxane / 14 h / 0 °C
5: 1.) NaOH, 2.) DCCD / 1.) dioxane, H2O, room temperature, 1 h, 2.) dioxane, from 0 grad C to room temperature
6: trifluoroacetic acid / 1 h / 0 °C
With
hydrogenchloride; sodium hydroxide; diphenyl phosphoryl azide; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
1,4-dioxane; water;
DOI:10.1016/S0040-4039(00)83967-2