1-<2-ethyl>-3-piperidinecarboxamide

Base Information

Chemical Name:1-<2-ethyl>-3-piperidinecarboxamide
CAS No.:143838-14-6
Molecular Formula:C₂₁H₂₄Cl₂N₂O₂
Molecular Weight:407.34
Hs Code.:

1-<2-<bis(4-chlorophenyl)methoxy>ethyl>-3-piperidinecarboxamide

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<2-ethyl>-3-piperidinecarboxamide

Chemical Property:

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Technology Process of 1-<2-ethyl>-3-piperidinecarboxamide

There total 5 articles about 1-<2-ethyl>-3-piperidinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-97-1
4,4'-dichlorobenzophenone

: 143838-14-6
1-<2-ethyl>-3-piperidinecarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: conc. H₂SO₄ / toluene / 2 h / 85 - 90 °C

2: K₂CO₃ / acetonitrile / 15 h / Heating

3: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

4: 1.) carbonyldiimidazole, 2.) NH₃(g) / 1.) THF, reflux, 24 h, 2.) THF, reflux, 20 h

With lithium hydroxide; sulfuric acid; ammonia; potassium carbonate; 1,1'-carbonyldiimidazole; In methanol; toluene; acetonitrile;
DOI:10.1021/jm00100a032

Reference yield:

: 221916-05-8
1-bromo-2-[bis(4-chlorophenyl)methoxy]ethane

: 143838-14-6
1-<2-ethyl>-3-piperidinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetonitrile / 15 h / Heating

2: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

3: 1.) carbonyldiimidazole, 2.) NH₃(g) / 1.) THF, reflux, 24 h, 2.) THF, reflux, 20 h

With lithium hydroxide; ammonia; potassium carbonate; 1,1'-carbonyldiimidazole; In methanol; acetonitrile;
DOI:10.1021/jm00100a032

Reference yield:

: 110283-43-7
1-<2-ethyl>-3-piperidinecarboxylic acid ethyl ester

: 143838-14-6
1-<2-ethyl>-3-piperidinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

2: 1.) carbonyldiimidazole, 2.) NH₃(g) / 1.) THF, reflux, 24 h, 2.) THF, reflux, 20 h

With lithium hydroxide; ammonia; 1,1'-carbonyldiimidazole; In methanol;
DOI:10.1021/jm00100a032