DL-tetra-O-acetyl-(1,3,5/2,4)-5-bromomethyl-1,2,3,4-cyclohexanetetrol

Base Information

Chemical Name:DL-tetra-O-acetyl-(1,3,5/2,4)-5-bromomethyl-1,2,3,4-cyclohexanetetrol
CAS No.:80065-31-2
Molecular Formula:C₁₅H₂₁BrO₈
Molecular Weight:409.231
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of DL-tetra-O-acetyl-(1,3,5/2,4)-5-bromomethyl-1,2,3,4-cyclohexanetetrol

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Technology Process of DL-tetra-O-acetyl-(1,3,5/2,4)-5-bromomethyl-1,2,3,4-cyclohexanetetrol

There total 3 articles about DL-tetra-O-acetyl-(1,3,5/2,4)-5-bromomethyl-1,2,3,4-cyclohexanetetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 10226-79-6,16656-57-8,16802-99-6,52079-86-4,60594-30-1,60594-31-2,64625-67-8,74560-70-6,74561-02-7,74561-06-1,74561-11-8,77209-45-1,90694-06-7,90695-22-0,94943-06-3,94943-07-4,97372-12-8,97372-20-8,97372-27-5,97372-29-7,102629-12-9,105017-73-0,105017-80-9,105368-83-0,108813-47-4,108813-49-6,108866-23-5,115184-61-7,115184-64-0
DL-penta-O-acetyl-(1,3,5/2,4)-5-hydroxymethyl-1,2,3,4-cyclohexanetetrol

: 80065-31-2,80124-74-9
DL-tetra-O-acetyl-(1,3,5/2,4)-5-bromomethyl-1,2,3,4-cyclohexanetetrol

Guidance literature:: With hydrogen bromide; In acetic acid; at 80 ℃; for 16h;
DOI:10.1246/bcsj.54.2739

Reference yield:

: 74766-78-2,96291-86-0,115225-42-8
3,4-di-O-acetyl-1,5-anhydro-6-bromo-2,6-dideoxy-5a-carba-DL-arabino-hex-1-enitol

: 80065-30-1
DL-trans-di-acetoxy-5-bromomethyl-2-cyclohexenone

: 80065-31-2,80124-74-9
DL-tetra-O-acetyl-(1,2,4/3,5)-5-bromomethyl-1,2,3,4-cyclohexanetetrol

Guidance literature:: With pyridine; osmium(VIII) oxide; dihydrogen peroxide; acetic anhydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) t-butyl alcohol, 30 deg, 24 h;
DOI:10.1246/bcsj.54.2739

Reference yield:

: 108-24-7
acetic anhydride

: 74766-78-2,96291-86-0,115225-42-8
3,4-di-O-acetyl-1,5-anhydro-6-bromo-2,6-dideoxy-5a-carba-DL-arabino-hex-1-enitol

: 80065-30-1
DL-trans-di-acetoxy-5-bromomethyl-2-cyclohexenone

: 80065-31-2,80124-74-9
DL-tetra-O-acetyl-(1,2,4/3,5)-5-bromomethyl-1,2,3,4-cyclohexanetetrol

Guidance literature:: With pyridine; osmium(VIII) oxide; dihydrogen peroxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) t-butyl alcohol, 25 deg, overnight;
DOI:10.1246/bcsj.54.2739